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Abstract

The crystal structure was solved by direct methods. Fuel matrix least squares refinement with all atoms, except H atoms, treated anisotropically gave an R value of 0.043. The coordination geometry about the uranium ion is pseudo-octahedral with one eta**5-C-9H-7 ligand and one coordinated H-4f (THF) molecule occupying transaxial positions, and the other H-4f molecule and three C1 atoms occupying equatorial positions.

Additional information

Authors: SPIRLET M R JRC KARLSRUHE ESTAB. (GERMANY) GOFFART J UNIVERSITE DE LIEGE (BELGIUM) , JRC KARLSRUHE ESTAB. (GERMANY);UNIVERSITE DE LIEGE (BELGIUM)
Bibliographic Reference: ACTA CRYSTALLOGRAPHICA, VOL. C39 (1983), PP. 1041-1043
Record Number: 1989122029500 / Last updated on: 1987-01-01
Category: PUBLICATION
Available languages: en