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  • Synthesis, characterization and investigation of the bonding in hydrotris(1-pyrazolyl)borato-technetium(VII)trioxide and hydrotris(3,5-dimethyl-1-pyrazolyl)borato-technetium(VII) trioxide


The compounds [HB(Pz)(3)]TcO(3) and [HB(3,5-Me(2)Pz)(3)]TcO(3) were synthesised by reaction of Tc(2)O(7) with K[HB(Pz)(3)] and Na[HB(3,5-Me(2)Pz)(3)] in THF. The IR, 1H NMR, UV, and EI-MS spectroscopic data are reported and discussed.

Additional information

Authors: JOACHIM J E ET AL., Forschungszentrum Karlsruhe GmbH (DE);APOSTOLIDIS C, JRC Karlsruhe (DE);KANELLAKOPULOS B, Anorganisch Chemisches Institut der Universität, Heidelberg (DE)
Bibliographic Reference: Article: Zeitschrift für Naturforschung (1993) 48b, pp. 227-229
Record Number: 199310961 / Last updated on: 1994-11-29
Original language: de
Available languages: de