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Abstract

To serve as a measurement standard, a (certified) reference material must be stable. For this purpose, the material should undergo stability testing after it has been prepared. This paper looks at the statistical aspects of stability testing. Essentially, these studies can be described with analysis of variance statistics, including variant regression analysis. The latter is used in practice for both trend analysis and for the development of expressions for extrapolations. Extrapolation of stability data is briefly touched upon, as far as the combined standard uncertainty of the reference material is concerned. There are different options to validate the extrapolations made from initial stability studies, and some of them might influence the uncertainty of the reference material and/or the shelf-life. The latter is the more commonly observed consequence of what is called ôstability monitoringö.

Additional information

Authors: VAN DER VEEN A.M.H, Nederlands Meetinstituut , Delft (NL);LINSINGER T.P.J, EC-JRC, Institute for Reference Materials and Measurements, Geel (BE);LAMBERTY A, EC-JRC, Institute for Reference Materials and Measurements, Geel (BE);PAUWELS J, EC-JRC, Institute for Reference Materials and Measurements, Geel (BE)
Bibliographic Reference: An article published in: ACQUAL (2001) 6, pp.257-263
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