In relation to the objectives and work plan set out in the project, we have carried out the following activities and achieved the following objectives.
Creation of a modern reference collection of plants:
• I have collected 10 arbustibos taxa for the modern reference collection, separated by their different parts: leaves, fruit, inflorescence and wood.
• I trained in the identification of these taxa in their environment, understanding their ecology and differentiating their different parts.
Sampling of Middle Pleistocene deposits
• I sampled the two sequences included in the project, Sima del Elefante and La Cansaladeta, following the anti-contamination protocols required by the protocols for chemical analysis of sediments.
• I was able to carry out continuous and representative sampling of the units analysed for subsequent analysis and I also learnt how to take samples for chemical analysis. I also learnt the importance of blanks in this type of analysis and the criteria to follow to ensure they are valid for the proposed analyses.
Biomarker analysis
• I analysed a total of 120 samples from the two sites to obtain qualitative and quantitative results for PAHs.
• This activity involved intensive training in basic chemistry, analytical chemistry, preparation of calibrations, preparation of deuterated compounds, preparation of sediment samples, extraction of analytes from sediment samples and obtaining results using gas chromatography-mass spectrometry. This training took place at the University of the Basque Country under the supervision of Prof. Asier Vallejo and lasted 5 months.
Phytolith analysis
• Carrying out the analysis of the 120 samples to obtain the phytoliths.
• I learnt to analyse contexts from the Middle Pleistocene, with low preservation and conservation of these microparticles.
Data Integration
• This activity involved reviewing the entire event at the sites studied, activating stalled analyses and encouraging the inclusion of new analyses, searching for researchers who could carry them out, sampling materials and coordinating a relevant group of researchers, together with the directors of the sites.
• A systematic collection was made of all the available bibliography; other analyses were carried out, such as palaeomagnetic analyses of the sediments, taphonomic analyses of the fauna, molecular analyses of the bones, macroscopic and experimental analyses of the burnt and unburnt lithic tools, micromorphological analyses and pH analyses of the sediments. For my part, I carried out analyses not included in the proposal, such as the determination of n-alkane values and FTR analyses of the sediments. We have also started a ground-breaking experimental project to understand how PAHs are deposited and preserved in relation to a flat combustion structure such as may have occurred in the deposits studied. We have also started a pioneering experimental project that will help us understand how PAHs are deposited and preserved in relation to a flat combustion structure such as the one that could have occurred in the deposits studied. We have also started a ground-breaking experimental project to understand how PAHs are deposited and preserved in relation to a flat combustion structure such as may have occurred in the deposits studied.