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Enantioenriched carboxylic acids from alkyl boronic esters through copper catalyzed CO2 fixation

Project description

Green chemistry with CO2 fixation

Traditional methods for synthesising chiral carboxylic acids rely on processes like hydrogenation and hydroxycarbonylation, which often lack efficiency and sustainability. A direct, catalytic approach using CO2 offers a greener alternative but remains largely underdeveloped. With the support of the Marie Skłodowska-Curie Actions programme, the CO2PPER project aims to revolutionise this field by leveraging stable alkylboronic esters in copper-catalysed carboxylation reactions. This method promises to overcome barriers in CO2 fixation, enabling the efficient production of enantioenriched chiral carboxylic acids. By using copper catalysts, known for their cost-effectiveness and low energy requirements, CO2PPER introduces an innovative, environmentally friendly strategy that advances CO2 valorisation while supporting sustainable chemical synthesis.

Objective

CO2PPER aims to explore a comprehensive method for the under-investigated catalytic CO2 fixation in asymmetric carboxylation reactions to produce chiral carboxylic acids. Unlike traditional methods that rely on asymmetric hydrogenation of α,β-unsaturated acids and hydroxycarbonylation of alkenes, catalytic CO2 fixation provides a direct and environmentally preferable alternative. Despite recent efforts in creating new chiral ligands to manage reactivity and selectivity, developing a universal catalytic carboxylation using CO2 remains an unsolved problem. CO2PPER proposes a novel approach by employing stable and easily accessible sterodefined alkylboronic esters in metal-catalyzed carboxylations to prepare a broad range of enantioenriched chiral carboxylic acids. The CO2 insertion will be achieved by the use of abundant and inexpensive copper-catalysts, taking advantage of the lowest energy barrier for CO2 insertion into a M-C bond. This project will significantly contribute to the advancement of the CO2-valorization framework and presents an innovative green methodology for chiral carboxylic acid synthesis.

Coordinator

UNIVERSIDAD AUTONOMA DE MADRID
Net EU contribution
€ 165 312,96
Address
CALLE EINSTEIN 3 CIUDAD UNIV CANTOBLANCO RECTORADO
28049 Madrid
Spain

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Region
Comunidad de Madrid Comunidad de Madrid Madrid
Activity type
Higher or Secondary Education Establishments
Links
Total cost
No data