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Cross-sectorial real-time sensing, advanced control and optimisation of batch processes saving energy and raw materials

Deliverables

Final model layout as a guide/tutorial for interested parties outside of RECOBA consortium

Final model layout as a guide/tutorial for interested parties outside of RECOBA consortium (M35; BFI)

A report on application of acoustic sensors for real-time properties sensing in different batch processes

A report on application of acoustic sensors for real-time properties sensing in different batch processes.

Report about the results of the comparison between conventional practice and new methods

Report about the results of the comparison between conventional practice and new methods (M36; BFI)

Report on performance of FBG fibre optical temperature measurement in refractories

Report on performance of FBG fibre optical temperature measurement in refractories

Ecobalance of the real-time controlled polymerisation, steel and silicon alloys process

Ecobalance of the real-time controlled polymerisation, steel and silicon alloys process (M32; BASF, TKSE, ELKEM)

Report about the results of the comparison between conventional practice and new practice

Report about the results of the comparison between conventional practice and new practice (M36; BASF)

Report on cross-sectorial transferability

Report on cross-sectorial transferability (M36; CYB)

Final report about the evaluation of the project

Final report about the evaluation of the project (M36; BFI)

Application of imaging methods (using optical and electromagnetic methods) in real-time properties measurements across batch processing methods. A cross-sectorial report

Application of imaging methods (using optical and electromagnetic methods) in real-time properties measurements across batch processing methods. A cross-sectorial report

Report on Raman spectroscopic monitoring of emulsion polymerisation with particle size and morphology information

Report on Raman spectroscopic monitoring of emulsion polymerisation with particle size and morphology information (M18; UCAM)

Symposium for process industry with high process temperatures

Symposium for process industry with high process temperatures (M24; BFI)

Kick-off exploitation workshop

Kick-off exploitation workshop (M6; CYB)

Midterm dissemination event: exploitation workshop 2

Midterm dissemination event: exploitation workshop 2 (M20; BASF)

Release of project web-site

Release of project web-site (M3; BASF)

Press release including a project leaflet

Press release including a project leaflet (M4; BASF)

Acoustic sensor for particle morphology monitoring (for different generation of sensors)

Acoustic sensor for particle morphology monitoring (M12, M18, M30 for different generation of sensors; UCAM)

Selection of best technology for temperature monitoring of solidification process

Selection of best technology for temperature monitoring of solidification process (M20; ELKEM)

Pilot scale verification of AMLDS and selection of most suitable system

Pilot scale verification of AMLDS and selection of most suitable system (M24; ELKEM)

Selection of two automated metal level detection systems (AMLDS) for testing in pilot scale

Selection of two automated metal level detection systems (AMLDS) for testing in pilot scale (M16; ELKEM)

Knowledge about temperature development in gas stirred ladle treatment batch process

Knowledge about temperature development in gas stirred ladle treatment batch process (M30; MINK)

Pilot scale test of ladle refractory temperature monitoring system

Pilot scale test of ladle refractory temperature monitoring system (M28; ELKEM)

Pilot-scale/industrial scale test of temperature monitoring of solidification process

Pilot-scale/industrial scale test of temperature monitoring of solidification process (M30; ELKEM)

Knowledge about temperature development in vacuum degassing batch process

Knowledge about temperature development in vacuum degassing batch process (M30; TKSE)

Event-triggered through process optimisation methods for the control of a chain of batch processes

Event-triggered through process optimisation methods for the control of a chain of batch processes (M24; BFI)

Selection of best technology for automated ladle refractory temperature monitoring

Selection of best technology for automated ladle refractory temperature monitoring (M18; ELKEM)

Set of evaluation criteria for the technical evaluation of different components and the overall results of the integrated process control

Set of evaluation criteria for the technical evaluation of different components and the overall results of the integrated process control (M32; BFI)

Detailed dynamic process model for both processes

Detailed dynamic process model for both processes (M30, BFI)

New developed sensors applicable for steelmaking processes

New developed sensors applicable for steelmaking processes (M18; MINK)

Coverage efficiency sensor to monitor temperature loss of high-temperature fluid by radiation

Coverage efficiency sensor to monitor temperature loss of high-temperature fluid by radiation

Fibre optical temperature sensor for monitoring temperature development of high-temperature fluids during batch processing

Fibre optical temperature sensor for monitoring temperature development of high-temperature fluids during batch processing

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Publications

Study the effect of reaction condition on the morphology of structured polymer particles in latexes

Author(s): Noushin Rajabalinia, Shaghayegh Hamzehlou, Jose R Leiza, Jose M Asua
Published in: Study the effect of reaction condition on the morphology of structured polymer particles in latexes, 2016

Shear-induced Coagulation in Stabilized Dispersions: Modeling by Discrete Element Method

Author(s): Martin Kroupa, Michal Vonka, Juraj Kosek
Published in: IACIS, 2015

Expected impact and an overview about progress in advanced process control of emulsion copolymerization

Author(s): L. Šeda, E. Jahns, A. Mhamdi, A. Mitsos, P. Joy, S. Hamzehlou, J. R. Leiza, J. M. Asua, N. Rajabalinia, J. Kosek, T. Chaloupka, M. Kroupa, M. DeMiguel-Ramos, A. J. Flewitt, A. Lapkin, J. Suberu, F. Gjertsen, P. Singstad
Published in: CHISA/PRES 2016, 2016

Optimization of dynamic systems with rigorous path constraint satisifaction

Author(s): Johannes M.M. Faust, Jun Fu, Benoit Chachuat, Alexander Mitsos
Published in: ESCAPE26, 2016

Real-time hybrid Monte Carlo method for modelling of 4 monomer semi-batch emulsion copolymerization

Author(s): T. Chaloupka, A. Zubov, Juraj Kosek
Published in: CHISA 2016, 2016

Skull formation in dynamic modelling of silicon refining

Author(s): Ellen Nordgard-Hansen, Kjetil Hildal
Published in: International Federation of Automatic Control (IFAC), Issue 17th, 2016

Local Optimization of Dynamic Systems with Guaranteed Feasibility of Path Constraints

Author(s): Johannes M. M. Faust, Jun Fu, Benoˆıt Chachuat, Alexander Mitsos
Published in: AIChE, 2015, 2015

Optimization with Dynamic Systems Embedded with Guaranteed Satisfaction of Path Constraints

Author(s): Johannes M. M. Faust, Jun Fu, Benoˆıt Chachuat, Alexander Mitsos
Published in: AC.CES 2015, Issue June 15, 2015

Real time sensing, dynamic modelling and advanced control of melt temperature in liquid steelmaking

Author(s): Bernd Kleimt, Tobias Kordel, Andreas Wolff, Sabine Will, Michael Skorianz, Mark Potter, Torsten Lamp, Herbert Köchner
Published in: Proceedings of the 3rd European Steel Technology and Application Days 2017, ESTAD 2017, 2017

Viscosity and Stability of Concentrated Colloidal Latexes Modeled by Discrete Element Method

Author(s): M. Kroupa, M. Vonka, M. Soos, J. Kosek
Published in: PRE 2016, 2016

Real-time hybrid Monte Carlo method for modelling of 4-monomer semi-batch emulsion copolymerization

Author(s): T.Chaloupka, A. Zubov, J. Kosek
Published in: WPPRE 2016, 2016

Coagulation and Fouling in Stabilized Colloidal Dispersions: Building a Predictive Model Based on First Principles

Author(s): M. Kroupa, M. Vonka, M. Soos, J. Kosek
Published in: International Conference on Chemical Technology, 2016

Dynamic model for on-line control of 4-monomer semi-batch emulsion copolymerization

Author(s): T.Chaloupka, A. Zubov, J. Kosek
Published in: Danube Vltava Sava Polymer Meeting, 2015

Real-time process optimisation by a model based on hybrid Monte Carlo method in semi-batch emulsion copolymerization

Author(s): T.Chaloupka, A. Zubov, J. Kosek
Published in: International Conference of Slovak Society of Chem. Eng., 2016

Modelling of concentrated colloidal dispersions using Discrete Element Method: stability, rheology and size of clusters

Author(s): M. Kroupa, M. Vonka, M. Soos, J. Kosek
Published in: 6th International Colloids Conference, 2016

On-line control and optimization for intensification of emulsion copolymerization reactors

Author(s): A. Zubov, R. Pokorny, P. Matuska, J. Kosek
Published in: International Conference on Chemical Technology, 2015

Use of Hybrid Monte-Carlo Models in Online Control of Product Quality in Emulsion Copolymerization

Author(s): A. Zubov, T. Chaloupka, J. Kosek
Published in: MaCKiE workshop, 2015

On-line optimization and control of emulsion copolymerization reactors

Author(s): J. Kosek, A. Zubov, R. Pokorny, T. Chaloupka
Published in: CHISA, 2015

"""Modeling the size and structure of clusters produced by shear-induced coagulation"" "

Author(s): M. Kroupa, M. Vonka, M. Soos, J. Kosek
Published in: ESCRE, 2015

Real-time hybrid Monte Carlo method for modelling of 4-monomer semi-batch emulsion copolymerization

Author(s): T.Chaloupka, A. Zubov, J. Kosek
Published in: PRE 2016, 2016

A new approach for mathematical modelling of the dynamic development of particle morphology

Author(s): Shaghayegh Hamzehlou; Jose Ramon Leiza; José M. Asua
Published in: PRE 2016, 2016

Optimization of dynamic systems with rigorous path constraint satisfaction

Author(s): Johannes M.M. Faust, Jun Fu, Benoît Chachuat, Alexander Mitsos
Published in: 26th European Symposium on Computer Aided Process Engineering, 2016, Page(s) 643-648
DOI: 10.1016/B978-0-444-63428-3.50112-0

Real-time Hybrid Monte Carlo Method for Modelling of 4 Monomer Semi-Batch Emulsion Copolymerization

Author(s): Tomas Chaloupka, Alexandr Zubov, Juraj Kosek
Published in: 27th European Symposium on Computer Aided Process Engineering, 2017, Page(s) 259-264
DOI: 10.1016/b978-0-444-63965-3.50045-3

Utilizing the Discrete Element Method for the Modeling of Viscosity in Concentrated Suspensions

Author(s): Martin Kroupa, Michal Vonka, Miroslav Soos, Juraj Kosek
Published in: Langmuir, Issue 32/33, 2016, Page(s) 8451-8460, ISSN 0743-7463
DOI: 10.1021/acs.langmuir.6b02335

Slip on a particle surface as the possible origin of shear thinning in non-Brownian suspensions

Author(s): Martin Kroupa, Miroslav Soos, Juraj Kosek
Published in: Physical Chemistry Chemical Physics, Issue 19/8, 2017, Page(s) 5979-5984, ISSN 1463-9076
DOI: 10.1039/C6CP07666A

Probing Coagulation and Fouling in Colloidal Dispersions with Viscosity Measurements: in-silico Proof of Concept

Author(s): Martin Kroupa, Michal Vonka, Miroslav Soos, Juraj Kosek
Published in: Advances in Polymer Science, 2017, Page(s) 1-22, ISSN 0065-3195
DOI: 10.1007/12_2017_17

Carbon nanotube isolation layer enhancing in-liquid quality-factors of thin film bulk acoustic wave resonators for gravimetric sensing

Author(s): G. Rughoobur, H. Sugime, M. DeMiguel-Ramos, T. Mirea, S. Zheng, J. Robertson, E. Iborra, A. J. Flewitt
Published in: Sensors and Actuators B, 2018, ISSN 0925-4005

Gravimetric sensors operating at 1.1 GHz based on inclined c -axis ZnO grown on textured Al electrodes

Author(s): G. Rughoobur, M. DeMiguel-Ramos, J.-M. Escolano, E. Iborra, and A. J. Flewitt
Published in: Scientific Reports, 2017, Page(s) 1367, ISSN 2045-2322

Room temperature sputtering of inclined c-axis ZnO for shear mode solidly mounted resonators

Author(s): G. Rughoobur, M. DeMiguel-Ramos, T. Mirea, M. Clement, J. Olivares, B. Díaz-Durán, J. Sangrador, I. Miele, W. I. Milne, E. Iborra, A. J. Flewitt
Published in: Applied Physics Letters, Issue 108/3, 2016, Page(s) 034103, ISSN 0003-6951
DOI: 10.1063/1.4940683

A new approach for mathematical modelling of the dynamic development of particle morphology

Author(s): Shaghayegh Hamzehlou; Jose Ramon Leiza; José M. Asua
Published in: Chemical Engineering Journal, 2016, ISSN 1385-8947