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European Training Network for Continuous Sonication and Microwave Reactors

Deliverables

1 COSMIC Symposium

1 COSMIC Symposium

1 COSMIC Summer School

1 COSMIC Summer School

First paper by ESR14-15

First paper by ESR14-15

Second paper by ESR10-13

Second paper by ESR10-13

Newsletters

Two newsletters (including policy statements), one in M24 and one in M48.

First paper by ESR5-9

First paper by ESR5-9

First paper by ESR1-4

First paper by ESR1-4

First paper by ESR10-13

First paper by ESR10-13

Final report on COSMIC project

Final report on COSMIC project

Second paper by ESR5-9

Second paper by ESR5-9

Special Issue Chemical Engineering and Processing: Process Intensification

Special Issue Chemical Engineering and Processing: Process Intensification

Second paper by ESR14-15

Second paper by ESR14-15

Second paper by ESR1-4

Second paper by ESR1-4

Promo videos

Two promo videos, one in M8 and one in M46

Website (external part)

Website (external part)

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Publications

Continuous flow synthesis of menthol via tandem cyclisation–hydrogenation of citronellal catalysed by scrap catalytic converters

Author(s): Alessio Zuliani, Camilla Maria Cova, Roberta Manno, Victor Sebastian, Antonio A. Romero, Rafael Luque
Published in: Green Chemistry, 22/2, 2020, Page(s) 379-387, ISSN 1463-9262
Publisher: Royal Society of Chemistry
DOI: 10.1039/c9gc03299a

Co-precipitation synthesis of stable iron oxide nanoparticles with NaOH: New insights and continuous production via flow chemistry

Author(s): Maximilian O. Besenhard, Alec P. LaGrow, Aden Hodzic, Manfred Kriechbaum, Luca Panariello, Giorgio Bais, Katerina Loizou, Spyridon Damilos, M. Margarida Cruz, Nguyen Thi Kim Thanh, Asterios Gavriilidis
Published in: Chemical Engineering Journal, 399, 2020, Page(s) 125740, ISSN 1385-8947
Publisher: Elsevier BV
DOI: 10.1016/j.cej.2020.125740

Cavitation bubble dynamics and sonochemiluminescence activity inside sonicated submerged flow tubes

Author(s): Busra Ekim Sarac, Dwayne Savio Stephens, Julian Eisener, Juan Manuel Rosselló, Robert Mettin
Published in: Chemical Engineering and Processing - Process Intensification, 150, 2020, Page(s) 107872, ISSN 0255-2701
Publisher: Elsevier BV
DOI: 10.1016/j.cep.2020.107872

Scrap waste automotive converters as efficient catalysts for the continuous-flow hydrogenations of biomass derived chemicals

Author(s): Camilla Maria Cova, Alessio Zuliani, Roberta Manno, Victor Sebastian, Rafael Luque
Published in: Green Chemistry, 22/4, 2020, Page(s) 1414-1423, ISSN 1463-9262
Publisher: Royal Society of Chemistry
DOI: 10.1039/C9GC04091A

Regeneration of Raney®-Nickel Catalyst for the Synthesis of High-Value Amino-Ester Renewable Monomers

Author(s): Ana Soutelo-Maria, Jean-Luc Dubois, Jean-Luc Couturier, Magali Brebion, Giancarlo Cravotto
Published in: Catalysts, 10/2, 2020, Page(s) 229, ISSN 2073-4344
Publisher: Multidisciplinary Digital Publishing Institute (MDPI)
DOI: 10.3390/catal10020229

On the Effect of Secondary Nucleation on Deracemization through Temperature Cycles

Author(s): Fabio Cameli, Joop H. ter Horst, René R. E. Steendam, Christos Xiouras, Georgios D. Stefanidis
Published in: Chemistry – A European Journal, 26/6, 2020, Page(s) 1344-1354, ISSN 0947-6539
Publisher: John Wiley & Sons Ltd.
DOI: 10.1002/chem.201904239

Life cycle assessment and cost evaluation of emerging technologies at early stages: The case of continuous flow synthesis of Rufinamide

Author(s): Fabio Grimaldi, Gerardo A. Leon Izeppi, Dirk Kirschneck, Paola Lettieri, Marc Escribà‐Gelonch, Volker Hessel
Published in: Journal of Advanced Manufacturing and Processing, 2/2, 2020, ISSN 2637-403X
Publisher: Wiley
DOI: 10.1002/amp2.10043

Effects of ultrasonic irradiation on crystallization kinetics, morphological and structural properties of zeolite FAU

Author(s): Heidy Ramirez Mendoza, Jeroen Jordens, Mafalda Valdez Lancinha Pereira, Cécile Lutz, Tom Van Gerven
Published in: Ultrasonics Sonochemistry, 64, 2020, Page(s) 105010, ISSN 1350-4177
Publisher: Elsevier BV
DOI: 10.1016/j.ultsonch.2020.105010

Continuous Ultrasonic Reactors: Design, Mechanism and Application

Author(s): Zhengya Dong, Claire Delacour, Keiran Mc Carogher, Aniket Pradip Udepurkar, Simon Kuhn
Published in: Materials, 13/2, 2020, Page(s) 344, ISSN 1996-1944
Publisher: MDPI Open Access Publishing
DOI: 10.3390/ma13020344

Highly reproducible, high-yield flow synthesis of gold nanoparticles based on a rational reactor design exploiting the reduction of passivated Au( iii )

Author(s): Luca Panariello, Spyridon Damilos, Hendrik du Toit, Gaowei Wu, Anand N. P. Radhakrishnan, Ivan P. Parkin, Asterios Gavriilidis
Published in: Reaction Chemistry & Engineering, 5/4, 2020, Page(s) 663-676, ISSN 2058-9883
Publisher: Royal Society of Chemistry
DOI: 10.1039/c9re00469f

Economic risk assessment using Monte Carlo simulation for the production of azelaic acid and pelargonic acid from vegetable oils

Author(s): Gerardo Antonio De Leon Izeppi, Jean-Luc Dubois, Antonin Balle, Ana Soutelo-Maria
Published in: Industrial Crops and Products, 150, 2020, Page(s) 112411, ISSN 0926-6690
Publisher: Elsevier BV
DOI: 10.1016/j.indcrop.2020.112411

Theoretical Study of the Scalability of a Sonicated Continuous Crystallizer for the Production of Aspirin

Author(s): Symeon V. Savvopoulos, Mohammed N. Hussain, Tom Van Gerven, Simon Kuhn
Published in: Industrial & Engineering Chemistry Research, 59/45, 2020, Page(s) 19952-19963, ISSN 0888-5885
Publisher: American Chemical Society
DOI: 10.1021/acs.iecr.0c03975

Ligand Enabled Palladium–Catalysed Through‐Space C‐H Bond Activation via a Carbopalladation/1,4‐Pd Migration/C‐H Functionalization Sequence

Author(s): Su Chen, Prabhat Ranjan, Nagarajan Ramkumar, Luc Van Meervelt, Erik V. Van der Eycken, Upendra K. Sharma
Published in: Chemistry – A European Journal, 2020, ISSN 0947-6539
Publisher: John Wiley & Sons Ltd.
DOI: 10.1002/chem.202001582

Combining the Ugi-azide multicomponent reaction and rhodium(III)-catalyzed annulation for the synthesis of tetrazole-isoquinolone/pyridone hybrids

Author(s): Gerardo M Ojeda, Prabhat Ranjan, Pavel Fedoseev, Lisandra Amable, Upendra K Sharma, Daniel G Rivera, Erik V Van der Eycken
Published in: Beilstein Journal of Organic Chemistry, 15, 2019, Page(s) 2447-2457, ISSN 1860-5397
Publisher: Beilstein-Institut
DOI: 10.3762/bjoc.15.237

Anticipatory life cycle assessment of gold nanoparticles production: Comparison of milli-continuous flow and batch synthesis

Author(s): Fabio Grimaldi, Martina Pucciarelli, Asterios Gavriilidis, Peter Dobson, Paola Lettieri
Published in: Journal of Cleaner Production, 269, 2020, Page(s) 122335, ISSN 0959-6526
Publisher: Elsevier BV
DOI: 10.1016/j.jclepro.2020.122335

Continuous Microwave-Assisted Synthesis of Silver Nanoclusters Confined in Mesoporous SBA-15: Application in Alkyne Cyclizations

Author(s): Roberta Manno, Prabhat Ranjan, Victor Sebastian, Reyes Mallada, Silvia Irusta, Upendra K. Sharma, Erik V. Van der Eycken, Jesús Santamaria
Published in: Chemistry of Materials, 32/7, 2020, Page(s) 2874-2883, ISSN 0897-4756
Publisher: American Chemical Society
DOI: 10.1021/acs.chemmater.9b04935

Efficient and Environmentally Friendly Microwave-Assisted Synthesis of Catalytically Active Magnetic Metallic Ni Nanoparticles

Author(s): Alessio Zuliani, Alina M. Balu, Rafael Luque
Published in: ACS Sustainable Chemistry & Engineering, 5/12, 2017, Page(s) 11584-11587, ISSN 2168-0485
Publisher: American Chemical Society
DOI: 10.1021/acssuschemeng.7b02945

Advances in Nanocatalyst Design for Biofuel Production

Author(s): Alessio Zuliani, Francisco Ivars, Rafael Luque
Published in: ChemCatChem, 10/9, 2018, Page(s) 1968-1981, ISSN 1867-3880
Publisher: Wiley - VCH Verlag GmbH & CO. KGaA
DOI: 10.1002/cctc.201701712

Microwave-assisted valorization of pig bristles: towards visible light photocatalytic chalcocite composites

Author(s): Alessio Zuliani, Mario J. Muñoz-Batista, Rafael Luque
Published in: Green Chemistry, 20/13, 2018, Page(s) 3001-3007, ISSN 1463-9262
Publisher: Royal Society of Chemistry
DOI: 10.1039/C8GC00669E

Modelling the synthesis of nanoparticles in continuous microreactors: The role of diffusion and residence time distribution on nanoparticle characteristics

Author(s): Luca Panariello, Luca Mazzei, Asterios Gavriilidis
Published in: Chemical Engineering Journal, 350, 2018, Page(s) 1144-1154, ISSN 1385-8947
Publisher: Elsevier BV
DOI: 10.1016/j.cej.2018.03.167

Intensified deracemization via rapid microwave-assisted temperature cycling

Author(s): Fabio Cameli, Christos Xiouras, Georgios D. Stefanidis
Published in: CrystEngComm, 20/21, 2018, Page(s) 2897-2901, ISSN 1466-8033
Publisher: Royal Society of Chemistry
DOI: 10.1039/c8ce00575c

Ex Situ Generation of Sulfuryl Fluoride for the Synthesis of Aryl Fluorosulfates

Author(s): Cedrick Veryser, Joachim Demaerel, Vidmantas Bieliu̅nas, Philippe Gilles, Wim M. De Borggraeve
Published in: Organic Letters, 19/19, 2017, Page(s) 5244-5247, ISSN 1523-7060
Publisher: American Chemical Society
DOI: 10.1021/acs.orglett.7b02522

Novel Applications of Microbial Fuel Cells in Sensors and Biosensors

Author(s): Francisco Ivars-Barceló, Alessio Zuliani, Marjan Fallah, Mehrdad Mashkour, Mostafa Rahimnejad, Rafael Luque
Published in: Applied Sciences, 8/7, 2018, Page(s) 1184, ISSN 2076-3417
Publisher: MDPI
DOI: 10.3390/app8071184

Microwave-assisted preparation of Ag/Ag 2 S carbon hybrid structures from pig bristles as efficient HER catalysts

Author(s): Camilla Maria Cova, Alessio Zuliani, Alain R. Puente Santiago, Alvaro Caballero, Mario J. Muñoz-Batista, Rafael Luque
Published in: Journal of Materials Chemistry A, 6/43, 2018, Page(s) 21516-21523, ISSN 2050-7488
Publisher: Royal Society of Chemistry
DOI: 10.1039/C8TA06417B

Oxidative Cleavage of Fatty Acid Derivatives for Monomer Synthesis

Author(s): Ana Soutelo-Maria, Jean-Luc Dubois, Jean-Luc Couturier, Giancarlo Cravotto
Published in: Catalysts, 8/10, 2018, Page(s) 464, ISSN 2073-4344
Publisher: Multidisciplinary Digital Publishing Institute (MDPI)
DOI: 10.3390/catal8100464

Heterogeneously Catalyzed Synthesis of Imidazolones via Cycloisomerizations of Propargylic Ureas Using Ag and Au/Al SBA-15 Systems

Author(s): Alessio Zuliani, Prabhat Ranjan, Rafael Luque, Erik V. Van der Eycken
Published in: ACS Sustainable Chemistry & Engineering, 7/5, 2019, Page(s) 5568-5575, ISSN 2168-0485
Publisher: American Chemical Society
DOI: 10.1021/acssuschemeng.9b00198

Preliminary economic assessment of a polymer production plant in batch and continuous manufacturing

Author(s): DE LEON IZEPPI, GERARDO ANTONIO; DREXLER, CHRISTIAN; KIRSCHNECK, DIRK
Published in: Chimica Oggi - Chemistry Today 36(5) 35-39, 36(5), 2018, Page(s) 36-39, ISSN 0392-839X
Publisher: Teknoscienze s.r.l.
DOI: 10.5281/zenodo.1584963

110th Anniversary: Nucleation of Ag Nanoparticles in Helical Microfluidic Reactor. Comparison between Microwave and Conventional Heating

Author(s): Roberta Manno, Victor Sebastian, Reyes Mallada, Jesús Santamaria
Published in: Industrial & Engineering Chemistry Research, 58/28, 2019, Page(s) 12702-12711, ISSN 0888-5885
Publisher: American Chemical Society
DOI: 10.1021/acs.iecr.9b01460

Pulsed ultrasound for temperature control and clogging prevention in micro-reactors

Author(s): Claire Delacour, Cecile Lutz, Simon Kuhn
Published in: Ultrasonics Sonochemistry, 55, 2019, Page(s) 67-74, ISSN 1350-4177
Publisher: Elsevier BV
DOI: 10.1016/j.ultsonch.2019.03.012

Sonochemically-Promoted Preparation of Silica-Anchored Cyclodextrin Derivatives for Efficient Copper Catalysis

Author(s): Katia Martina, Federica Calsolaro, Alessio Zuliani, Gloria Berlier, Fernando Chávez-Rivas, Maria Jesus Moran, Rafael Luque, Giancarlo Cravotto
Published in: Molecules, 24/13, 2019, Page(s) 2490, ISSN 1420-3049
Publisher: Multidisciplinary Digital Publishing Institute (MDPI)
DOI: 10.3390/molecules24132490

Sonocrystallisation: Observations, theories and guidelines

Author(s): Jeroen Jordens, Bjorn Gielen, Christos Xiouras, Mohammed Noorul Hussain, Georgios D. Stefanidis, Leen C.J. Thomassen, Leen Braeken, Tom Van Gerven
Published in: Chemical Engineering and Processing - Process Intensification, 139, 2019, Page(s) 130-154, ISSN 0255-2701
Publisher: Elsevier BV
DOI: 10.1016/j.cep.2019.03.017

A Mathematical Model of the Ultrasound-Assisted Continuous Tubular Crystallization of Aspirin

Author(s): Symeon V. Savvopoulos, Mohammed N. Hussain, Jeroen Jordens, Steffen Waldherr, Tom Van Gerven, Simon Kuhn
Published in: Crystal Growth & Design, 19/9, 2019, Page(s) 5111-5122, ISSN 1528-7483
Publisher: American Chemical Society
DOI: 10.1021/acs.cgd.9b00466

Enhancing pharmaceutical crystallization in a flow crystallizer with ultrasound: Anti-solvent crystallization

Author(s): M.N. Hussain, J. Jordens, J.J. John, L. Braeken, T. Van Gerven
Published in: Ultrasonics Sonochemistry, 59, 2019, Page(s) 104743, ISSN 1350-4177
Publisher: Elsevier BV
DOI: 10.1016/j.ultsonch.2019.104743

Glycerol: An Optimal Hydrogen Source for Microwave-Promoted Cu-Catalyzed Transfer Hydrogenation of Nitrobenzene to Aniline

Author(s): Maria Jesus Moran, Katia Martina, Georgios D. Stefanidis, Jeroen Jordens, Tom Van Gerven, Vincent Goovaerts, Maela Manzoli, Carlo Groffils, Giancarlo Cravotto
Published in: Frontiers in Chemistry, 8, 2020, ISSN 2296-2646
Publisher: Frontiers
DOI: 10.3389/fchem.2020.00034

Tuneable Copper Catalysed Transfer Hydrogenation of Nitrobenzenes to Aniline or Azo Derivatives

Author(s): Maria Jesus Moran, Katia Martina, Francesca Baricco, Silvia Tagliapietra, Maela Manzoli, Giancarlo Cravotto
Published in: Advanced Synthesis & Catalysis, 362, 2020, ISSN 1615-4150
Publisher: John Wiley & Sons Ltd.
DOI: 10.1002/adsc.202000127

A model for the formation of gold nanoparticles in the citrate synthesis method

Author(s): Emmanuel Agunloye, Luca Panariello, Asterios Gavriilidis, Luca Mazzei
Published in: Chemical Engineering Science, 191, 2018, Page(s) 318-331, ISSN 0009-2509
Publisher: Pergamon Press Ltd.
DOI: 10.1016/j.ces.2018.06.046

Introduction of Aryl Fluorosulfates into the Realm of Catellani Reaction Substrates

Author(s): Vidmantas Bieliu̅nas, Wim M. De Borggraeve
Published in: The Journal of Organic Chemistry, 84/23, 2019, Page(s) 15706-15717, ISSN 0022-3263
Publisher: American Chemical Society
DOI: 10.1021/acs.joc.9b02352

Multistep Solvent-Free 3 m 2 Footprint Pilot Miniplant for the Synthesis of Annual Half-Ton Rufinamide Precursor

Author(s): Marc Escribà-Gelonch, Gerardo Antonio de Leon Izeppi, Dirk Kirschneck, Volker Hessel
Published in: ACS Sustainable Chemistry & Engineering, 7/20, 2019, Page(s) 17237-17251, ISSN 2168-0485
Publisher: American Chemical Society
DOI: 10.1021/acssuschemeng.9b03931

Metal‐Free Dearomatization: Direct Access to Spiroindol(en)ines in Batch and Continuous‐Flow

Author(s): Prabhat Ranjan, Gerardo M. Ojeda, Upendra K. Sharma, Erik V. Van der Eycken
Published in: Chemistry – A European Journal, 25/10, 2019, Page(s) 2442-2446, ISSN 0947-6539
Publisher: John Wiley & Sons Ltd.
DOI: 10.1002/chem.201805945

A Sustainable Approach for the Synthesis of Catalytically Active Peroxidase-Mimic ZnS Catalysts

Author(s): Camilla M. Cova, Alessio Zuliani, Mario J. Muñoz-Batista, Rafael Luque
Published in: ACS Sustainable Chemistry & Engineering, 7/1, 2018, Page(s) 1300-1307, ISSN 2168-0485
Publisher: American Chemical Society
DOI: 10.1021/acssuschemeng.8b04968

Ultrasound as a tool for polymorph control and high yield in flow crystallization

Author(s): Mohammed Noorul Hussain, Jeroen Jordens, Simon Kuhn, Leen Braeken, Tom Van Gerven
Published in: Chemical Engineering Journal, 2020, Page(s) 127272, ISSN 1385-8947
Publisher: Elsevier BV
DOI: 10.1016/j.cej.2020.127272

Synthetic guidelines for the precision engineering of gold nanoparticles

Author(s): Jakub W Trzciński, Luca Panariello, Maximilian O Besenhard, Ye Yang, Asterios Gavriilidis, Stefan Guldin
Published in: Current Opinion in Chemical Engineering, 29, 2020, Page(s) 59-66, ISSN 2211-3398
Publisher: Elsevier BV
DOI: 10.1016/j.coche.2020.05.004

Process intensified anti-solvent crystallization of o-aminobenzoic acid via sonication and flow

Author(s): Mohammed Noorul Hussain, Stijn Baeten, Jeroen Jordens, Leen Braeken, Tom Van Gerven
Published in: Chemical Engineering and Processing - Process Intensification, 149, 2020, Page(s) 107823, ISSN 0255-2701
Publisher: Elsevier BV
DOI: 10.1016/j.cep.2020.107823

Sustainable Protocol for the Reduction of Nitroarenes by Heterogeneous Au@SBA‐15 with NaBH 4 under Flow Conditions

Author(s): Francesco Ferlin, Tommaso Giannoni, Alessio Zuliani, Oriana Piermatti, Rafael Luque, Luigi Vaccaro
Published in: ChemSusChem, 12/13, 2019, Page(s) 3178-3184, ISSN 1864-5631
Publisher: Wiley - V C H Verlag GmbbH & Co.
DOI: 10.1002/cssc.201802359

Continuous flow synthesis of zeolite FAU in an oscillatory baffled reactor

Author(s): Heidy Ramirez Mendoza, Mafalda Valdez Lancinha Pereira, Tom Van Gerven, Cécile Lutz
Published in: Journal of Advanced Manufacturing and Processing, 2/2, 2020, ISSN 2637-403X
Publisher: Wiley
DOI: 10.1002/amp2.10038

A Modular Millifluidic Platform for the Synthesis of Iron Oxide Nanoparticles with Control over Dissolved Gas and Flow Configuration

Author(s): Luca Panariello, Gaowei Wu, Maximilian O. Besenhard, Katerina Loizou, Liudmyla Storozhuk, Nguyen Thi Kim Thanh, Asterios Gavriilidis
Published in: Materials, 13/4, 2020, Page(s) 1019, ISSN 1996-1944
Publisher: MDPI Open Access Publishing
DOI: 10.3390/ma13041019

Efficient Ru-based scrap waste automotive converter catalysts for the continuous-flow selective hydrogenation of cinnamaldehyde

Author(s): Camilla Maria Cova, Alessio Zuliani, Mario J. Muñoz-Batista, Rafael Luque
Published in: Green Chemistry, 21/17, 2019, Page(s) 4712-4722, ISSN 1463-9262
Publisher: Royal Society of Chemistry
DOI: 10.1039/c9gc01596e

Microwave-assisted synthesis of nanocatalysts in batch conditions

Author(s): Zuliani, Alessio
Published in: 1, 2019
Publisher: University of Cordoba, UCOPress

ULTRASOUND-ASSISTED SYNTHESIS OF ZEOLITE CATALYSTS

Author(s): Heidy RAMIREZ MENDOZA
Published in: 2020
Publisher: KU leuven

Can the use of captured CO2 lower the environmental impacts of formate production?

Author(s): Pucciarelli, M; Grimaldi, F; Paulillo, A; Lettieri, P
Published in: Proceedings of Chemeca 2019: Chemical Engineering Megatrends and Elements, Chemeca 2019, 2019, Page(s) 324-335
Publisher: Informit

Flow Chemistry for the Synthesis of Heterocycles

Author(s): Joachim Demaerel, Vidmantas Bieliūnas, Wim M. De Borggraeve
Published in: Functionalization of Heteroarenes Under Continuous Flow, Volume 56, 2018, Page(s) 237-317, ISBN 3319-943286
Publisher: Springer International Publishing
DOI: 10.1007/7081_2018_22

Continuous Synthesis of Gold Nanoparticles in Micro- and Milli-fluidic Systems

Author(s): Huang, H.; Du Toit, H.; Panariello, L.; Mazzei, L.; Gavriilidis, A.
Published in: In: Kumar, C, (ed.) Chemistry of Nanomaterials: A Practical Guide. Volume 1: Metallic Nanomaterials (Part A). (pp. 157-220). De Gruyter: Berlin, Germany. (2018), 2, 2019
Publisher: De Gruyter
DOI: 10.1515/9783110345100-004