European Training Network for Continuous Sonication and Microwave Reactors

Risultati finali

1 COSMIC Symposium
1 COSMIC Summer School

First paper by ESR14-15
Second paper by ESR10-13
Newsletters

Two newsletters (including policy statements), one in M24 and one in M48.

First paper by ESR5-9
First paper by ESR1-4
First paper by ESR10-13
Final report on COSMIC project
Second paper by ESR5-9
Special Issue Chemical Engineering and Processing: Process Intensification
Second paper by ESR14-15
Second paper by ESR1-4

Promo videos

Two promo videos, one in M8 and one in M46

Website (external part)

Pubblicazioni

Continuous flow synthesis of menthol via tandem cyclisation–hydrogenation of citronellal catalysed by scrap catalytic converters

Autori: Alessio Zuliani, Camilla Maria Cova, Roberta Manno, Victor Sebastian, Antonio A. Romero, Rafael Luque
Pubblicato in: Green Chemistry, Numero 22/2, 2020, Pagina/e 379-387, ISSN 1463-9262
Editore: Royal Society of Chemistry
DOI: 10.1039/c9gc03299a

Co-precipitation synthesis of stable iron oxide nanoparticles with NaOH: New insights and continuous production via flow chemistry

Autori: Maximilian O. Besenhard, Alec P. LaGrow, Aden Hodzic, Manfred Kriechbaum, Luca Panariello, Giorgio Bais, Katerina Loizou, Spyridon Damilos, M. Margarida Cruz, Nguyen Thi Kim Thanh, Asterios Gavriilidis
Pubblicato in: Chemical Engineering Journal, Numero 399, 2020, Pagina/e 125740, ISSN 1385-8947
Editore: Elsevier BV
DOI: 10.1016/j.cej.2020.125740

Cavitation bubble dynamics and sonochemiluminescence activity inside sonicated submerged flow tubes

Autori: Busra Ekim Sarac, Dwayne Savio Stephens, Julian Eisener, Juan Manuel Rosselló, Robert Mettin
Pubblicato in: Chemical Engineering and Processing - Process Intensification, Numero 150, 2020, Pagina/e 107872, ISSN 0255-2701
Editore: Elsevier BV
DOI: 10.1016/j.cep.2020.107872

Scrap waste automotive converters as efficient catalysts for the continuous-flow hydrogenations of biomass derived chemicals

Autori: Camilla Maria Cova, Alessio Zuliani, Roberta Manno, Victor Sebastian, Rafael Luque
Pubblicato in: Green Chemistry, Numero 22/4, 2020, Pagina/e 1414-1423, ISSN 1463-9262
Editore: Royal Society of Chemistry
DOI: 10.1039/C9GC04091A

Regeneration of Raney®-Nickel Catalyst for the Synthesis of High-Value Amino-Ester Renewable Monomers

Autori: Ana Soutelo-Maria, Jean-Luc Dubois, Jean-Luc Couturier, Magali Brebion, Giancarlo Cravotto
Pubblicato in: Catalysts, Numero 10/2, 2020, Pagina/e 229, ISSN 2073-4344
Editore: Multidisciplinary Digital Publishing Institute (MDPI)
DOI: 10.3390/catal10020229

On the Effect of Secondary Nucleation on Deracemization through Temperature Cycles

Autori: Fabio Cameli, Joop H. ter Horst, René R. E. Steendam, Christos Xiouras, Georgios D. Stefanidis
Pubblicato in: Chemistry – A European Journal, Numero 26/6, 2020, Pagina/e 1344-1354, ISSN 0947-6539
Editore: John Wiley & Sons Ltd.
DOI: 10.1002/chem.201904239

Life cycle assessment and cost evaluation of emerging technologies at early stages: The case of continuous flow synthesis of Rufinamide

Autori: Fabio Grimaldi, Gerardo A. Leon Izeppi, Dirk Kirschneck, Paola Lettieri, Marc Escribà‐Gelonch, Volker Hessel
Pubblicato in: Journal of Advanced Manufacturing and Processing, Numero 2/2, 2020, ISSN 2637-403X
Editore: Wiley
DOI: 10.1002/amp2.10043

Effects of ultrasonic irradiation on crystallization kinetics, morphological and structural properties of zeolite FAU

Autori: Heidy Ramirez Mendoza, Jeroen Jordens, Mafalda Valdez Lancinha Pereira, Cécile Lutz, Tom Van Gerven
Pubblicato in: Ultrasonics Sonochemistry, Numero 64, 2020, Pagina/e 105010, ISSN 1350-4177
Editore: Elsevier BV
DOI: 10.1016/j.ultsonch.2020.105010

Continuous Ultrasonic Reactors: Design, Mechanism and Application

Autori: Zhengya Dong, Claire Delacour, Keiran Mc Carogher, Aniket Pradip Udepurkar, Simon Kuhn
Pubblicato in: Materials, Numero 13/2, 2020, Pagina/e 344, ISSN 1996-1944
Editore: MDPI Open Access Publishing
DOI: 10.3390/ma13020344

Highly reproducible, high-yield flow synthesis of gold nanoparticles based on a rational reactor design exploiting the reduction of passivated Au( iii )

Autori: Luca Panariello, Spyridon Damilos, Hendrik du Toit, Gaowei Wu, Anand N. P. Radhakrishnan, Ivan P. Parkin, Asterios Gavriilidis
Pubblicato in: Reaction Chemistry & Engineering, Numero 5/4, 2020, Pagina/e 663-676, ISSN 2058-9883
Editore: Royal Society of Chemistry
DOI: 10.1039/c9re00469f

Economic risk assessment using Monte Carlo simulation for the production of azelaic acid and pelargonic acid from vegetable oils

Autori: Gerardo Antonio De Leon Izeppi, Jean-Luc Dubois, Antonin Balle, Ana Soutelo-Maria
Pubblicato in: Industrial Crops and Products, Numero 150, 2020, Pagina/e 112411, ISSN 0926-6690
Editore: Elsevier BV
DOI: 10.1016/j.indcrop.2020.112411

Theoretical Study of the Scalability of a Sonicated Continuous Crystallizer for the Production of Aspirin

Autori: Symeon V. Savvopoulos, Mohammed N. Hussain, Tom Van Gerven, Simon Kuhn
Pubblicato in: Industrial & Engineering Chemistry Research, Numero 59/45, 2020, Pagina/e 19952-19963, ISSN 0888-5885
Editore: American Chemical Society
DOI: 10.1021/acs.iecr.0c03975

Ligand Enabled Palladium–Catalysed Through‐Space C‐H Bond Activation via a Carbopalladation/1,4‐Pd Migration/C‐H Functionalization Sequence

Autori: Su Chen, Prabhat Ranjan, Nagarajan Ramkumar, Luc Van Meervelt, Erik V. Van der Eycken, Upendra K. Sharma
Pubblicato in: Chemistry – A European Journal, 2020, ISSN 0947-6539
Editore: John Wiley & Sons Ltd.
DOI: 10.1002/chem.202001582

Combining the Ugi-azide multicomponent reaction and rhodium(III)-catalyzed annulation for the synthesis of tetrazole-isoquinolone/pyridone hybrids

Autori: Gerardo M Ojeda, Prabhat Ranjan, Pavel Fedoseev, Lisandra Amable, Upendra K Sharma, Daniel G Rivera, Erik V Van der Eycken
Pubblicato in: Beilstein Journal of Organic Chemistry, Numero 15, 2019, Pagina/e 2447-2457, ISSN 1860-5397
Editore: Beilstein-Institut
DOI: 10.3762/bjoc.15.237

Anticipatory life cycle assessment of gold nanoparticles production: Comparison of milli-continuous flow and batch synthesis

Autori: Fabio Grimaldi, Martina Pucciarelli, Asterios Gavriilidis, Peter Dobson, Paola Lettieri
Pubblicato in: Journal of Cleaner Production, Numero 269, 2020, Pagina/e 122335, ISSN 0959-6526
Editore: Elsevier BV
DOI: 10.1016/j.jclepro.2020.122335

Continuous Microwave-Assisted Synthesis of Silver Nanoclusters Confined in Mesoporous SBA-15: Application in Alkyne Cyclizations

Autori: Roberta Manno, Prabhat Ranjan, Victor Sebastian, Reyes Mallada, Silvia Irusta, Upendra K. Sharma, Erik V. Van der Eycken, Jesús Santamaria
Pubblicato in: Chemistry of Materials, Numero 32/7, 2020, Pagina/e 2874-2883, ISSN 0897-4756
Editore: American Chemical Society
DOI: 10.1021/acs.chemmater.9b04935

Efficient and Environmentally Friendly Microwave-Assisted Synthesis of Catalytically Active Magnetic Metallic Ni Nanoparticles

Autori: Alessio Zuliani, Alina M. Balu, Rafael Luque
Pubblicato in: ACS Sustainable Chemistry & Engineering, Numero 5/12, 2017, Pagina/e 11584-11587, ISSN 2168-0485
Editore: American Chemical Society
DOI: 10.1021/acssuschemeng.7b02945

Advances in Nanocatalyst Design for Biofuel Production

Autori: Alessio Zuliani, Francisco Ivars, Rafael Luque
Pubblicato in: ChemCatChem, Numero 10/9, 2018, Pagina/e 1968-1981, ISSN 1867-3880
Editore: Wiley - VCH Verlag GmbH & CO. KGaA
DOI: 10.1002/cctc.201701712

Microwave-assisted valorization of pig bristles: towards visible light photocatalytic chalcocite composites

Autori: Alessio Zuliani, Mario J. Muñoz-Batista, Rafael Luque
Pubblicato in: Green Chemistry, Numero 20/13, 2018, Pagina/e 3001-3007, ISSN 1463-9262
Editore: Royal Society of Chemistry
DOI: 10.1039/C8GC00669E

Modelling the synthesis of nanoparticles in continuous microreactors: The role of diffusion and residence time distribution on nanoparticle characteristics

Autori: Luca Panariello, Luca Mazzei, Asterios Gavriilidis
Pubblicato in: Chemical Engineering Journal, Numero 350, 2018, Pagina/e 1144-1154, ISSN 1385-8947
Editore: Elsevier BV
DOI: 10.1016/j.cej.2018.03.167

Intensified deracemization via rapid microwave-assisted temperature cycling

Autori: Fabio Cameli, Christos Xiouras, Georgios D. Stefanidis
Pubblicato in: CrystEngComm, Numero 20/21, 2018, Pagina/e 2897-2901, ISSN 1466-8033
Editore: Royal Society of Chemistry
DOI: 10.1039/c8ce00575c

Ex Situ Generation of Sulfuryl Fluoride for the Synthesis of Aryl Fluorosulfates

Autori: Cedrick Veryser, Joachim Demaerel, Vidmantas Bieliu̅nas, Philippe Gilles, Wim M. De Borggraeve
Pubblicato in: Organic Letters, Numero 19/19, 2017, Pagina/e 5244-5247, ISSN 1523-7060
Editore: American Chemical Society
DOI: 10.1021/acs.orglett.7b02522

Novel Applications of Microbial Fuel Cells in Sensors and Biosensors

Autori: Francisco Ivars-Barceló, Alessio Zuliani, Marjan Fallah, Mehrdad Mashkour, Mostafa Rahimnejad, Rafael Luque
Pubblicato in: Applied Sciences, Numero 8/7, 2018, Pagina/e 1184, ISSN 2076-3417
Editore: MDPI
DOI: 10.3390/app8071184

Microwave-assisted preparation of Ag/Ag 2 S carbon hybrid structures from pig bristles as efficient HER catalysts

Autori: Camilla Maria Cova, Alessio Zuliani, Alain R. Puente Santiago, Alvaro Caballero, Mario J. Muñoz-Batista, Rafael Luque
Pubblicato in: Journal of Materials Chemistry A, Numero 6/43, 2018, Pagina/e 21516-21523, ISSN 2050-7488
Editore: Royal Society of Chemistry
DOI: 10.1039/C8TA06417B

Oxidative Cleavage of Fatty Acid Derivatives for Monomer Synthesis

Autori: Ana Soutelo-Maria, Jean-Luc Dubois, Jean-Luc Couturier, Giancarlo Cravotto
Pubblicato in: Catalysts, Numero 8/10, 2018, Pagina/e 464, ISSN 2073-4344
Editore: Multidisciplinary Digital Publishing Institute (MDPI)
DOI: 10.3390/catal8100464

Heterogeneously Catalyzed Synthesis of Imidazolones via Cycloisomerizations of Propargylic Ureas Using Ag and Au/Al SBA-15 Systems

Autori: Alessio Zuliani, Prabhat Ranjan, Rafael Luque, Erik V. Van der Eycken
Pubblicato in: ACS Sustainable Chemistry & Engineering, Numero 7/5, 2019, Pagina/e 5568-5575, ISSN 2168-0485
Editore: American Chemical Society
DOI: 10.1021/acssuschemeng.9b00198

Preliminary economic assessment of a polymer production plant in batch and continuous manufacturing

Autori: DE LEON IZEPPI, GERARDO ANTONIO; DREXLER, CHRISTIAN; KIRSCHNECK, DIRK
Pubblicato in: Chimica Oggi - Chemistry Today 36(5) 35-39, Numero 36(5), 2018, Pagina/e 36-39, ISSN 0392-839X
Editore: Teknoscienze s.r.l.
DOI: 10.5281/zenodo.1584963

110th Anniversary: Nucleation of Ag Nanoparticles in Helical Microfluidic Reactor. Comparison between Microwave and Conventional Heating

Autori: Roberta Manno, Victor Sebastian, Reyes Mallada, Jesús Santamaria
Pubblicato in: Industrial & Engineering Chemistry Research, Numero 58/28, 2019, Pagina/e 12702-12711, ISSN 0888-5885
Editore: American Chemical Society
DOI: 10.1021/acs.iecr.9b01460

Pulsed ultrasound for temperature control and clogging prevention in micro-reactors

Autori: Claire Delacour, Cecile Lutz, Simon Kuhn
Pubblicato in: Ultrasonics Sonochemistry, Numero 55, 2019, Pagina/e 67-74, ISSN 1350-4177
Editore: Elsevier BV
DOI: 10.1016/j.ultsonch.2019.03.012

Sonochemically-Promoted Preparation of Silica-Anchored Cyclodextrin Derivatives for Efficient Copper Catalysis

Autori: Katia Martina, Federica Calsolaro, Alessio Zuliani, Gloria Berlier, Fernando Chávez-Rivas, Maria Jesus Moran, Rafael Luque, Giancarlo Cravotto
Pubblicato in: Molecules, Numero 24/13, 2019, Pagina/e 2490, ISSN 1420-3049
Editore: Multidisciplinary Digital Publishing Institute (MDPI)
DOI: 10.3390/molecules24132490

Sonocrystallisation: Observations, theories and guidelines

Autori: Jeroen Jordens, Bjorn Gielen, Christos Xiouras, Mohammed Noorul Hussain, Georgios D. Stefanidis, Leen C.J. Thomassen, Leen Braeken, Tom Van Gerven
Pubblicato in: Chemical Engineering and Processing - Process Intensification, Numero 139, 2019, Pagina/e 130-154, ISSN 0255-2701
Editore: Elsevier BV
DOI: 10.1016/j.cep.2019.03.017

A Mathematical Model of the Ultrasound-Assisted Continuous Tubular Crystallization of Aspirin

Autori: Symeon V. Savvopoulos, Mohammed N. Hussain, Jeroen Jordens, Steffen Waldherr, Tom Van Gerven, Simon Kuhn
Pubblicato in: Crystal Growth & Design, Numero 19/9, 2019, Pagina/e 5111-5122, ISSN 1528-7483
Editore: American Chemical Society
DOI: 10.1021/acs.cgd.9b00466

Enhancing pharmaceutical crystallization in a flow crystallizer with ultrasound: Anti-solvent crystallization

Autori: M.N. Hussain, J. Jordens, J.J. John, L. Braeken, T. Van Gerven
Pubblicato in: Ultrasonics Sonochemistry, Numero 59, 2019, Pagina/e 104743, ISSN 1350-4177
Editore: Elsevier BV
DOI: 10.1016/j.ultsonch.2019.104743

Glycerol: An Optimal Hydrogen Source for Microwave-Promoted Cu-Catalyzed Transfer Hydrogenation of Nitrobenzene to Aniline

Autori: Maria Jesus Moran, Katia Martina, Georgios D. Stefanidis, Jeroen Jordens, Tom Van Gerven, Vincent Goovaerts, Maela Manzoli, Carlo Groffils, Giancarlo Cravotto
Pubblicato in: Frontiers in Chemistry, Numero 8, 2020, ISSN 2296-2646
Editore: Frontiers
DOI: 10.3389/fchem.2020.00034

Tuneable Copper Catalysed Transfer Hydrogenation of Nitrobenzenes to Aniline or Azo Derivatives

Autori: Maria Jesus Moran, Katia Martina, Francesca Baricco, Silvia Tagliapietra, Maela Manzoli, Giancarlo Cravotto
Pubblicato in: Advanced Synthesis & Catalysis, Numero 362, 2020, ISSN 1615-4150
Editore: John Wiley & Sons Ltd.
DOI: 10.1002/adsc.202000127

A model for the formation of gold nanoparticles in the citrate synthesis method

Autori: Emmanuel Agunloye, Luca Panariello, Asterios Gavriilidis, Luca Mazzei
Pubblicato in: Chemical Engineering Science, Numero 191, 2018, Pagina/e 318-331, ISSN 0009-2509
Editore: Pergamon Press Ltd.
DOI: 10.1016/j.ces.2018.06.046

Introduction of Aryl Fluorosulfates into the Realm of Catellani Reaction Substrates

Autori: Vidmantas Bieliu̅nas, Wim M. De Borggraeve
Pubblicato in: The Journal of Organic Chemistry, Numero 84/23, 2019, Pagina/e 15706-15717, ISSN 0022-3263
Editore: American Chemical Society
DOI: 10.1021/acs.joc.9b02352

Multistep Solvent-Free 3 m 2 Footprint Pilot Miniplant for the Synthesis of Annual Half-Ton Rufinamide Precursor

Autori: Marc Escribà-Gelonch, Gerardo Antonio de Leon Izeppi, Dirk Kirschneck, Volker Hessel
Pubblicato in: ACS Sustainable Chemistry & Engineering, Numero 7/20, 2019, Pagina/e 17237-17251, ISSN 2168-0485
Editore: American Chemical Society
DOI: 10.1021/acssuschemeng.9b03931

Metal‐Free Dearomatization: Direct Access to Spiroindol(en)ines in Batch and Continuous‐Flow

Autori: Prabhat Ranjan, Gerardo M. Ojeda, Upendra K. Sharma, Erik V. Van der Eycken
Pubblicato in: Chemistry – A European Journal, Numero 25/10, 2019, Pagina/e 2442-2446, ISSN 0947-6539
Editore: John Wiley & Sons Ltd.
DOI: 10.1002/chem.201805945

A Sustainable Approach for the Synthesis of Catalytically Active Peroxidase-Mimic ZnS Catalysts

Autori: Camilla M. Cova, Alessio Zuliani, Mario J. Muñoz-Batista, Rafael Luque
Pubblicato in: ACS Sustainable Chemistry & Engineering, Numero 7/1, 2018, Pagina/e 1300-1307, ISSN 2168-0485
Editore: American Chemical Society
DOI: 10.1021/acssuschemeng.8b04968

Ultrasound as a tool for polymorph control and high yield in flow crystallization

Autori: Mohammed Noorul Hussain, Jeroen Jordens, Simon Kuhn, Leen Braeken, Tom Van Gerven
Pubblicato in: Chemical Engineering Journal, 2020, Pagina/e 127272, ISSN 1385-8947
Editore: Elsevier BV
DOI: 10.1016/j.cej.2020.127272

Synthetic guidelines for the precision engineering of gold nanoparticles

Autori: Jakub W Trzciński, Luca Panariello, Maximilian O Besenhard, Ye Yang, Asterios Gavriilidis, Stefan Guldin
Pubblicato in: Current Opinion in Chemical Engineering, Numero 29, 2020, Pagina/e 59-66, ISSN 2211-3398
Editore: Elsevier BV
DOI: 10.1016/j.coche.2020.05.004

Process intensified anti-solvent crystallization of o-aminobenzoic acid via sonication and flow

Autori: Mohammed Noorul Hussain, Stijn Baeten, Jeroen Jordens, Leen Braeken, Tom Van Gerven
Pubblicato in: Chemical Engineering and Processing - Process Intensification, Numero 149, 2020, Pagina/e 107823, ISSN 0255-2701
Editore: Elsevier BV
DOI: 10.1016/j.cep.2020.107823

Sustainable Protocol for the Reduction of Nitroarenes by Heterogeneous Au@SBA‐15 with NaBH 4 under Flow Conditions

Autori: Francesco Ferlin, Tommaso Giannoni, Alessio Zuliani, Oriana Piermatti, Rafael Luque, Luigi Vaccaro
Pubblicato in: ChemSusChem, Numero 12/13, 2019, Pagina/e 3178-3184, ISSN 1864-5631
Editore: Wiley - V C H Verlag GmbbH & Co.
DOI: 10.1002/cssc.201802359

Continuous flow synthesis of zeolite FAU in an oscillatory baffled reactor

Autori: Heidy Ramirez Mendoza, Mafalda Valdez Lancinha Pereira, Tom Van Gerven, Cécile Lutz
Pubblicato in: Journal of Advanced Manufacturing and Processing, Numero 2/2, 2020, ISSN 2637-403X
Editore: Wiley
DOI: 10.1002/amp2.10038

A Modular Millifluidic Platform for the Synthesis of Iron Oxide Nanoparticles with Control over Dissolved Gas and Flow Configuration

Autori: Luca Panariello, Gaowei Wu, Maximilian O. Besenhard, Katerina Loizou, Liudmyla Storozhuk, Nguyen Thi Kim Thanh, Asterios Gavriilidis
Pubblicato in: Materials, Numero 13/4, 2020, Pagina/e 1019, ISSN 1996-1944
Editore: MDPI Open Access Publishing
DOI: 10.3390/ma13041019

Efficient Ru-based scrap waste automotive converter catalysts for the continuous-flow selective hydrogenation of cinnamaldehyde

Autori: Camilla Maria Cova, Alessio Zuliani, Mario J. Muñoz-Batista, Rafael Luque
Pubblicato in: Green Chemistry, Numero 21/17, 2019, Pagina/e 4712-4722, ISSN 1463-9262
Editore: Royal Society of Chemistry
DOI: 10.1039/c9gc01596e

Microwave-assisted synthesis of nanocatalysts in batch conditions

Autori: Zuliani, Alessio
Pubblicato in: Numero 1, 2019
Editore: University of Cordoba, UCOPress

ULTRASOUND-ASSISTED SYNTHESIS OF ZEOLITE CATALYSTS

Autori: Heidy RAMIREZ MENDOZA
Pubblicato in: 2020
Editore: KU leuven

Can the use of captured CO2 lower the environmental impacts of formate production?

Autori: Pucciarelli, M; Grimaldi, F; Paulillo, A; Lettieri, P
Pubblicato in: Proceedings of Chemeca 2019: Chemical Engineering Megatrends and Elements, Numero Chemeca 2019, 2019, Pagina/e 324-335
Editore: Informit

Flow Chemistry for the Synthesis of Heterocycles

Autori: Joachim Demaerel, Vidmantas Bieliūnas, Wim M. De Borggraeve
Pubblicato in: Functionalization of Heteroarenes Under Continuous Flow, Numero Volume 56, 2018, Pagina/e 237-317, ISBN 3319-943286
Editore: Springer International Publishing
DOI: 10.1007/7081_2018_22

Continuous Synthesis of Gold Nanoparticles in Micro- and Milli-fluidic Systems

Autori: Huang, H.; Du Toit, H.; Panariello, L.; Mazzei, L.; Gavriilidis, A.
Pubblicato in: In: Kumar, C, (ed.) Chemistry of Nanomaterials: A Practical Guide. Volume 1: Metallic Nanomaterials (Part A). (pp. 157-220). De Gruyter: Berlin, Germany. (2018), Numero 2, 2019
Editore: De Gruyter
DOI: 10.1515/9783110345100-004

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