European Training Network for Continuous Sonication and Microwave Reactors

Resultado final

1 COSMIC Symposium
1 COSMIC Summer School

First paper by ESR14-15
Second paper by ESR10-13
Newsletters

Two newsletters (including policy statements), one in M24 and one in M48.

First paper by ESR5-9
First paper by ESR1-4
First paper by ESR10-13
Final report on COSMIC project
Second paper by ESR5-9
Special Issue Chemical Engineering and Processing: Process Intensification
Second paper by ESR14-15
Second paper by ESR1-4

Promo videos

Two promo videos, one in M8 and one in M46

Website (external part)

Publicaciones

Continuous flow synthesis of menthol via tandem cyclisation–hydrogenation of citronellal catalysed by scrap catalytic converters

Autores: Alessio Zuliani, Camilla Maria Cova, Roberta Manno, Victor Sebastian, Antonio A. Romero, Rafael Luque
Publicado en: Green Chemistry, Edición 22/2, 2020, Página(s) 379-387, ISSN 1463-9262
Editor: Royal Society of Chemistry
DOI: 10.1039/c9gc03299a

Co-precipitation synthesis of stable iron oxide nanoparticles with NaOH: New insights and continuous production via flow chemistry

Autores: Maximilian O. Besenhard, Alec P. LaGrow, Aden Hodzic, Manfred Kriechbaum, Luca Panariello, Giorgio Bais, Katerina Loizou, Spyridon Damilos, M. Margarida Cruz, Nguyen Thi Kim Thanh, Asterios Gavriilidis
Publicado en: Chemical Engineering Journal, Edición 399, 2020, Página(s) 125740, ISSN 1385-8947
Editor: Elsevier BV
DOI: 10.1016/j.cej.2020.125740

Cavitation bubble dynamics and sonochemiluminescence activity inside sonicated submerged flow tubes

Autores: Busra Ekim Sarac, Dwayne Savio Stephens, Julian Eisener, Juan Manuel Rosselló, Robert Mettin
Publicado en: Chemical Engineering and Processing - Process Intensification, Edición 150, 2020, Página(s) 107872, ISSN 0255-2701
Editor: Elsevier BV
DOI: 10.1016/j.cep.2020.107872

Scrap waste automotive converters as efficient catalysts for the continuous-flow hydrogenations of biomass derived chemicals

Autores: Camilla Maria Cova, Alessio Zuliani, Roberta Manno, Victor Sebastian, Rafael Luque
Publicado en: Green Chemistry, Edición 22/4, 2020, Página(s) 1414-1423, ISSN 1463-9262
Editor: Royal Society of Chemistry
DOI: 10.1039/C9GC04091A

Regeneration of Raney®-Nickel Catalyst for the Synthesis of High-Value Amino-Ester Renewable Monomers

Autores: Ana Soutelo-Maria, Jean-Luc Dubois, Jean-Luc Couturier, Magali Brebion, Giancarlo Cravotto
Publicado en: Catalysts, Edición 10/2, 2020, Página(s) 229, ISSN 2073-4344
Editor: Multidisciplinary Digital Publishing Institute (MDPI)
DOI: 10.3390/catal10020229

On the Effect of Secondary Nucleation on Deracemization through Temperature Cycles

Autores: Fabio Cameli, Joop H. ter Horst, René R. E. Steendam, Christos Xiouras, Georgios D. Stefanidis
Publicado en: Chemistry – A European Journal, Edición 26/6, 2020, Página(s) 1344-1354, ISSN 0947-6539
Editor: John Wiley & Sons Ltd.
DOI: 10.1002/chem.201904239

Life cycle assessment and cost evaluation of emerging technologies at early stages: The case of continuous flow synthesis of Rufinamide

Autores: Fabio Grimaldi, Gerardo A. Leon Izeppi, Dirk Kirschneck, Paola Lettieri, Marc Escribà‐Gelonch, Volker Hessel
Publicado en: Journal of Advanced Manufacturing and Processing, Edición 2/2, 2020, ISSN 2637-403X
Editor: Wiley
DOI: 10.1002/amp2.10043

Effects of ultrasonic irradiation on crystallization kinetics, morphological and structural properties of zeolite FAU

Autores: Heidy Ramirez Mendoza, Jeroen Jordens, Mafalda Valdez Lancinha Pereira, Cécile Lutz, Tom Van Gerven
Publicado en: Ultrasonics Sonochemistry, Edición 64, 2020, Página(s) 105010, ISSN 1350-4177
Editor: Elsevier BV
DOI: 10.1016/j.ultsonch.2020.105010

Continuous Ultrasonic Reactors: Design, Mechanism and Application

Autores: Zhengya Dong, Claire Delacour, Keiran Mc Carogher, Aniket Pradip Udepurkar, Simon Kuhn
Publicado en: Materials, Edición 13/2, 2020, Página(s) 344, ISSN 1996-1944
Editor: MDPI Open Access Publishing
DOI: 10.3390/ma13020344

Highly reproducible, high-yield flow synthesis of gold nanoparticles based on a rational reactor design exploiting the reduction of passivated Au( iii )

Autores: Luca Panariello, Spyridon Damilos, Hendrik du Toit, Gaowei Wu, Anand N. P. Radhakrishnan, Ivan P. Parkin, Asterios Gavriilidis
Publicado en: Reaction Chemistry & Engineering, Edición 5/4, 2020, Página(s) 663-676, ISSN 2058-9883
Editor: Royal Society of Chemistry
DOI: 10.1039/c9re00469f

Economic risk assessment using Monte Carlo simulation for the production of azelaic acid and pelargonic acid from vegetable oils

Autores: Gerardo Antonio De Leon Izeppi, Jean-Luc Dubois, Antonin Balle, Ana Soutelo-Maria
Publicado en: Industrial Crops and Products, Edición 150, 2020, Página(s) 112411, ISSN 0926-6690
Editor: Elsevier BV
DOI: 10.1016/j.indcrop.2020.112411

Theoretical Study of the Scalability of a Sonicated Continuous Crystallizer for the Production of Aspirin

Autores: Symeon V. Savvopoulos, Mohammed N. Hussain, Tom Van Gerven, Simon Kuhn
Publicado en: Industrial & Engineering Chemistry Research, Edición 59/45, 2020, Página(s) 19952-19963, ISSN 0888-5885
Editor: American Chemical Society
DOI: 10.1021/acs.iecr.0c03975

Ligand Enabled Palladium–Catalysed Through‐Space C‐H Bond Activation via a Carbopalladation/1,4‐Pd Migration/C‐H Functionalization Sequence

Autores: Su Chen, Prabhat Ranjan, Nagarajan Ramkumar, Luc Van Meervelt, Erik V. Van der Eycken, Upendra K. Sharma
Publicado en: Chemistry – A European Journal, 2020, ISSN 0947-6539
Editor: John Wiley & Sons Ltd.
DOI: 10.1002/chem.202001582

Combining the Ugi-azide multicomponent reaction and rhodium(III)-catalyzed annulation for the synthesis of tetrazole-isoquinolone/pyridone hybrids

Autores: Gerardo M Ojeda, Prabhat Ranjan, Pavel Fedoseev, Lisandra Amable, Upendra K Sharma, Daniel G Rivera, Erik V Van der Eycken
Publicado en: Beilstein Journal of Organic Chemistry, Edición 15, 2019, Página(s) 2447-2457, ISSN 1860-5397
Editor: Beilstein-Institut
DOI: 10.3762/bjoc.15.237

Anticipatory life cycle assessment of gold nanoparticles production: Comparison of milli-continuous flow and batch synthesis

Autores: Fabio Grimaldi, Martina Pucciarelli, Asterios Gavriilidis, Peter Dobson, Paola Lettieri
Publicado en: Journal of Cleaner Production, Edición 269, 2020, Página(s) 122335, ISSN 0959-6526
Editor: Elsevier BV
DOI: 10.1016/j.jclepro.2020.122335

Continuous Microwave-Assisted Synthesis of Silver Nanoclusters Confined in Mesoporous SBA-15: Application in Alkyne Cyclizations

Autores: Roberta Manno, Prabhat Ranjan, Victor Sebastian, Reyes Mallada, Silvia Irusta, Upendra K. Sharma, Erik V. Van der Eycken, Jesús Santamaria
Publicado en: Chemistry of Materials, Edición 32/7, 2020, Página(s) 2874-2883, ISSN 0897-4756
Editor: American Chemical Society
DOI: 10.1021/acs.chemmater.9b04935

Efficient and Environmentally Friendly Microwave-Assisted Synthesis of Catalytically Active Magnetic Metallic Ni Nanoparticles

Autores: Alessio Zuliani, Alina M. Balu, Rafael Luque
Publicado en: ACS Sustainable Chemistry & Engineering, Edición 5/12, 2017, Página(s) 11584-11587, ISSN 2168-0485
Editor: American Chemical Society
DOI: 10.1021/acssuschemeng.7b02945

Advances in Nanocatalyst Design for Biofuel Production

Autores: Alessio Zuliani, Francisco Ivars, Rafael Luque
Publicado en: ChemCatChem, Edición 10/9, 2018, Página(s) 1968-1981, ISSN 1867-3880
Editor: Wiley - VCH Verlag GmbH & CO. KGaA
DOI: 10.1002/cctc.201701712

Microwave-assisted valorization of pig bristles: towards visible light photocatalytic chalcocite composites

Autores: Alessio Zuliani, Mario J. Muñoz-Batista, Rafael Luque
Publicado en: Green Chemistry, Edición 20/13, 2018, Página(s) 3001-3007, ISSN 1463-9262
Editor: Royal Society of Chemistry
DOI: 10.1039/C8GC00669E

Modelling the synthesis of nanoparticles in continuous microreactors: The role of diffusion and residence time distribution on nanoparticle characteristics

Autores: Luca Panariello, Luca Mazzei, Asterios Gavriilidis
Publicado en: Chemical Engineering Journal, Edición 350, 2018, Página(s) 1144-1154, ISSN 1385-8947
Editor: Elsevier BV
DOI: 10.1016/j.cej.2018.03.167

Intensified deracemization via rapid microwave-assisted temperature cycling

Autores: Fabio Cameli, Christos Xiouras, Georgios D. Stefanidis
Publicado en: CrystEngComm, Edición 20/21, 2018, Página(s) 2897-2901, ISSN 1466-8033
Editor: Royal Society of Chemistry
DOI: 10.1039/c8ce00575c

Ex Situ Generation of Sulfuryl Fluoride for the Synthesis of Aryl Fluorosulfates

Autores: Cedrick Veryser, Joachim Demaerel, Vidmantas Bieliu̅nas, Philippe Gilles, Wim M. De Borggraeve
Publicado en: Organic Letters, Edición 19/19, 2017, Página(s) 5244-5247, ISSN 1523-7060
Editor: American Chemical Society
DOI: 10.1021/acs.orglett.7b02522

Novel Applications of Microbial Fuel Cells in Sensors and Biosensors

Autores: Francisco Ivars-Barceló, Alessio Zuliani, Marjan Fallah, Mehrdad Mashkour, Mostafa Rahimnejad, Rafael Luque
Publicado en: Applied Sciences, Edición 8/7, 2018, Página(s) 1184, ISSN 2076-3417
Editor: MDPI
DOI: 10.3390/app8071184

Microwave-assisted preparation of Ag/Ag 2 S carbon hybrid structures from pig bristles as efficient HER catalysts

Autores: Camilla Maria Cova, Alessio Zuliani, Alain R. Puente Santiago, Alvaro Caballero, Mario J. Muñoz-Batista, Rafael Luque
Publicado en: Journal of Materials Chemistry A, Edición 6/43, 2018, Página(s) 21516-21523, ISSN 2050-7488
Editor: Royal Society of Chemistry
DOI: 10.1039/C8TA06417B

Oxidative Cleavage of Fatty Acid Derivatives for Monomer Synthesis

Autores: Ana Soutelo-Maria, Jean-Luc Dubois, Jean-Luc Couturier, Giancarlo Cravotto
Publicado en: Catalysts, Edición 8/10, 2018, Página(s) 464, ISSN 2073-4344
Editor: Multidisciplinary Digital Publishing Institute (MDPI)
DOI: 10.3390/catal8100464

Heterogeneously Catalyzed Synthesis of Imidazolones via Cycloisomerizations of Propargylic Ureas Using Ag and Au/Al SBA-15 Systems

Autores: Alessio Zuliani, Prabhat Ranjan, Rafael Luque, Erik V. Van der Eycken
Publicado en: ACS Sustainable Chemistry & Engineering, Edición 7/5, 2019, Página(s) 5568-5575, ISSN 2168-0485
Editor: American Chemical Society
DOI: 10.1021/acssuschemeng.9b00198

Preliminary economic assessment of a polymer production plant in batch and continuous manufacturing

Autores: DE LEON IZEPPI, GERARDO ANTONIO; DREXLER, CHRISTIAN; KIRSCHNECK, DIRK
Publicado en: Chimica Oggi - Chemistry Today 36(5) 35-39, Edición 36(5), 2018, Página(s) 36-39, ISSN 0392-839X
Editor: Teknoscienze s.r.l.
DOI: 10.5281/zenodo.1584963

110th Anniversary: Nucleation of Ag Nanoparticles in Helical Microfluidic Reactor. Comparison between Microwave and Conventional Heating

Autores: Roberta Manno, Victor Sebastian, Reyes Mallada, Jesús Santamaria
Publicado en: Industrial & Engineering Chemistry Research, Edición 58/28, 2019, Página(s) 12702-12711, ISSN 0888-5885
Editor: American Chemical Society
DOI: 10.1021/acs.iecr.9b01460

Pulsed ultrasound for temperature control and clogging prevention in micro-reactors

Autores: Claire Delacour, Cecile Lutz, Simon Kuhn
Publicado en: Ultrasonics Sonochemistry, Edición 55, 2019, Página(s) 67-74, ISSN 1350-4177
Editor: Elsevier BV
DOI: 10.1016/j.ultsonch.2019.03.012

Sonochemically-Promoted Preparation of Silica-Anchored Cyclodextrin Derivatives for Efficient Copper Catalysis

Autores: Katia Martina, Federica Calsolaro, Alessio Zuliani, Gloria Berlier, Fernando Chávez-Rivas, Maria Jesus Moran, Rafael Luque, Giancarlo Cravotto
Publicado en: Molecules, Edición 24/13, 2019, Página(s) 2490, ISSN 1420-3049
Editor: Multidisciplinary Digital Publishing Institute (MDPI)
DOI: 10.3390/molecules24132490

Sonocrystallisation: Observations, theories and guidelines

Autores: Jeroen Jordens, Bjorn Gielen, Christos Xiouras, Mohammed Noorul Hussain, Georgios D. Stefanidis, Leen C.J. Thomassen, Leen Braeken, Tom Van Gerven
Publicado en: Chemical Engineering and Processing - Process Intensification, Edición 139, 2019, Página(s) 130-154, ISSN 0255-2701
Editor: Elsevier BV
DOI: 10.1016/j.cep.2019.03.017

A Mathematical Model of the Ultrasound-Assisted Continuous Tubular Crystallization of Aspirin

Autores: Symeon V. Savvopoulos, Mohammed N. Hussain, Jeroen Jordens, Steffen Waldherr, Tom Van Gerven, Simon Kuhn
Publicado en: Crystal Growth & Design, Edición 19/9, 2019, Página(s) 5111-5122, ISSN 1528-7483
Editor: American Chemical Society
DOI: 10.1021/acs.cgd.9b00466

Enhancing pharmaceutical crystallization in a flow crystallizer with ultrasound: Anti-solvent crystallization

Autores: M.N. Hussain, J. Jordens, J.J. John, L. Braeken, T. Van Gerven
Publicado en: Ultrasonics Sonochemistry, Edición 59, 2019, Página(s) 104743, ISSN 1350-4177
Editor: Elsevier BV
DOI: 10.1016/j.ultsonch.2019.104743

Glycerol: An Optimal Hydrogen Source for Microwave-Promoted Cu-Catalyzed Transfer Hydrogenation of Nitrobenzene to Aniline

Autores: Maria Jesus Moran, Katia Martina, Georgios D. Stefanidis, Jeroen Jordens, Tom Van Gerven, Vincent Goovaerts, Maela Manzoli, Carlo Groffils, Giancarlo Cravotto
Publicado en: Frontiers in Chemistry, Edición 8, 2020, ISSN 2296-2646
Editor: Frontiers
DOI: 10.3389/fchem.2020.00034

Tuneable Copper Catalysed Transfer Hydrogenation of Nitrobenzenes to Aniline or Azo Derivatives

Autores: Maria Jesus Moran, Katia Martina, Francesca Baricco, Silvia Tagliapietra, Maela Manzoli, Giancarlo Cravotto
Publicado en: Advanced Synthesis & Catalysis, Edición 362, 2020, ISSN 1615-4150
Editor: John Wiley & Sons Ltd.
DOI: 10.1002/adsc.202000127

A model for the formation of gold nanoparticles in the citrate synthesis method

Autores: Emmanuel Agunloye, Luca Panariello, Asterios Gavriilidis, Luca Mazzei
Publicado en: Chemical Engineering Science, Edición 191, 2018, Página(s) 318-331, ISSN 0009-2509
Editor: Pergamon Press Ltd.
DOI: 10.1016/j.ces.2018.06.046

Introduction of Aryl Fluorosulfates into the Realm of Catellani Reaction Substrates

Autores: Vidmantas Bieliu̅nas, Wim M. De Borggraeve
Publicado en: The Journal of Organic Chemistry, Edición 84/23, 2019, Página(s) 15706-15717, ISSN 0022-3263
Editor: American Chemical Society
DOI: 10.1021/acs.joc.9b02352

Multistep Solvent-Free 3 m 2 Footprint Pilot Miniplant for the Synthesis of Annual Half-Ton Rufinamide Precursor

Autores: Marc Escribà-Gelonch, Gerardo Antonio de Leon Izeppi, Dirk Kirschneck, Volker Hessel
Publicado en: ACS Sustainable Chemistry & Engineering, Edición 7/20, 2019, Página(s) 17237-17251, ISSN 2168-0485
Editor: American Chemical Society
DOI: 10.1021/acssuschemeng.9b03931

Metal‐Free Dearomatization: Direct Access to Spiroindol(en)ines in Batch and Continuous‐Flow

Autores: Prabhat Ranjan, Gerardo M. Ojeda, Upendra K. Sharma, Erik V. Van der Eycken
Publicado en: Chemistry – A European Journal, Edición 25/10, 2019, Página(s) 2442-2446, ISSN 0947-6539
Editor: John Wiley & Sons Ltd.
DOI: 10.1002/chem.201805945

A Sustainable Approach for the Synthesis of Catalytically Active Peroxidase-Mimic ZnS Catalysts

Autores: Camilla M. Cova, Alessio Zuliani, Mario J. Muñoz-Batista, Rafael Luque
Publicado en: ACS Sustainable Chemistry & Engineering, Edición 7/1, 2018, Página(s) 1300-1307, ISSN 2168-0485
Editor: American Chemical Society
DOI: 10.1021/acssuschemeng.8b04968

Ultrasound as a tool for polymorph control and high yield in flow crystallization

Autores: Mohammed Noorul Hussain, Jeroen Jordens, Simon Kuhn, Leen Braeken, Tom Van Gerven
Publicado en: Chemical Engineering Journal, 2020, Página(s) 127272, ISSN 1385-8947
Editor: Elsevier BV
DOI: 10.1016/j.cej.2020.127272

Synthetic guidelines for the precision engineering of gold nanoparticles

Autores: Jakub W Trzciński, Luca Panariello, Maximilian O Besenhard, Ye Yang, Asterios Gavriilidis, Stefan Guldin
Publicado en: Current Opinion in Chemical Engineering, Edición 29, 2020, Página(s) 59-66, ISSN 2211-3398
Editor: Elsevier BV
DOI: 10.1016/j.coche.2020.05.004

Process intensified anti-solvent crystallization of o-aminobenzoic acid via sonication and flow

Autores: Mohammed Noorul Hussain, Stijn Baeten, Jeroen Jordens, Leen Braeken, Tom Van Gerven
Publicado en: Chemical Engineering and Processing - Process Intensification, Edición 149, 2020, Página(s) 107823, ISSN 0255-2701
Editor: Elsevier BV
DOI: 10.1016/j.cep.2020.107823

Sustainable Protocol for the Reduction of Nitroarenes by Heterogeneous Au@SBA‐15 with NaBH 4 under Flow Conditions

Autores: Francesco Ferlin, Tommaso Giannoni, Alessio Zuliani, Oriana Piermatti, Rafael Luque, Luigi Vaccaro
Publicado en: ChemSusChem, Edición 12/13, 2019, Página(s) 3178-3184, ISSN 1864-5631
Editor: Wiley - V C H Verlag GmbbH & Co.
DOI: 10.1002/cssc.201802359

Continuous flow synthesis of zeolite FAU in an oscillatory baffled reactor

Autores: Heidy Ramirez Mendoza, Mafalda Valdez Lancinha Pereira, Tom Van Gerven, Cécile Lutz
Publicado en: Journal of Advanced Manufacturing and Processing, Edición 2/2, 2020, ISSN 2637-403X
Editor: Wiley
DOI: 10.1002/amp2.10038

A Modular Millifluidic Platform for the Synthesis of Iron Oxide Nanoparticles with Control over Dissolved Gas and Flow Configuration

Autores: Luca Panariello, Gaowei Wu, Maximilian O. Besenhard, Katerina Loizou, Liudmyla Storozhuk, Nguyen Thi Kim Thanh, Asterios Gavriilidis
Publicado en: Materials, Edición 13/4, 2020, Página(s) 1019, ISSN 1996-1944
Editor: MDPI Open Access Publishing
DOI: 10.3390/ma13041019

Efficient Ru-based scrap waste automotive converter catalysts for the continuous-flow selective hydrogenation of cinnamaldehyde

Autores: Camilla Maria Cova, Alessio Zuliani, Mario J. Muñoz-Batista, Rafael Luque
Publicado en: Green Chemistry, Edición 21/17, 2019, Página(s) 4712-4722, ISSN 1463-9262
Editor: Royal Society of Chemistry
DOI: 10.1039/c9gc01596e

Microwave-assisted synthesis of nanocatalysts in batch conditions

Autores: Zuliani, Alessio
Publicado en: Edición 1, 2019
Editor: University of Cordoba, UCOPress

ULTRASOUND-ASSISTED SYNTHESIS OF ZEOLITE CATALYSTS

Autores: Heidy RAMIREZ MENDOZA
Publicado en: 2020
Editor: KU leuven

Can the use of captured CO2 lower the environmental impacts of formate production?

Autores: Pucciarelli, M; Grimaldi, F; Paulillo, A; Lettieri, P
Publicado en: Proceedings of Chemeca 2019: Chemical Engineering Megatrends and Elements, Edición Chemeca 2019, 2019, Página(s) 324-335
Editor: Informit

Flow Chemistry for the Synthesis of Heterocycles

Autores: Joachim Demaerel, Vidmantas Bieliūnas, Wim M. De Borggraeve
Publicado en: Functionalization of Heteroarenes Under Continuous Flow, Edición Volume 56, 2018, Página(s) 237-317, ISBN 3319-943286
Editor: Springer International Publishing
DOI: 10.1007/7081_2018_22

Continuous Synthesis of Gold Nanoparticles in Micro- and Milli-fluidic Systems

Autores: Huang, H.; Du Toit, H.; Panariello, L.; Mazzei, L.; Gavriilidis, A.
Publicado en: In: Kumar, C, (ed.) Chemistry of Nanomaterials: A Practical Guide. Volume 1: Metallic Nanomaterials (Part A). (pp. 157-220). De Gruyter: Berlin, Germany. (2018), Edición 2, 2019
Editor: De Gruyter
DOI: 10.1515/9783110345100-004

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