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Mechanochemistry: a unique opportunity for oxygen isotopic labelling and NMR spectroscopy

Pubblicazioni

From Operando Raman Mechanochemistry to “NMR Crystallography”: Understanding the Structures and Interconversion of Zn-Terephthalate Networks Using Selective 17O‑Labeling

Autori: César Leroy, Thomas-Xavier Métro, Ivan Hung, Zhehong Gan, Christel Gervais, Danielle Laurencin
Pubblicato in: Chemistry of Materials, 2022, ISSN 0897-4756
Editore: American Chemical Society
DOI: 10.1021/acs.chemmater.1c04132

Probing oxygen exchange between UiO‐66(Zr) MOF and water using <sup>17</sup>O solid‐state NMR

Autori: Florian Venel; Raynald Giovine; Danielle Laurencin; Jessica Špačková; Sébastien Mittelette; Thomas‐Xavier Métro; Christophe Volkringer; Olivier Lafon; Frédérique Pourpoint
Pubblicato in: https://hal.univ-lille.fr/hal-04480095, Issue 1, 2024, ISSN 0947-6539
Editore: John Wiley & Sons Ltd.
DOI: 10.1002/chem.202302731

Solvent-free synthesis of zeolites: New insights into the mechanism and non-mechanochemical route

Autori: Shadi Al-Nahari; Danielle Laurencin; Bruno Alonso
Pubblicato in: Microporous and Mesoporous Materials, Issue 350, 2023, Page(s) 112445, ISSN 1387-1811
Editore: Elsevier BV
DOI: 10.1016/j.micromeso.2023.112445

Labeling and Probing the Silica Surface Using Mechanochemistry and 17 O NMR Spectroscopy**

Autori: Chia‐Hsin Chen, Frederic Mentink‐Vigier, Julien Trébosc, Ieva Goldberga, Philippe Gaveau, Emilie Thomassot, Dinu Iuga, Mark E. Smith, Kuizhi Chen, Zhehong Gan, Nicolas Fabregue, Thomas‐Xavier Métro, Bruno Alonso, Danielle Laurencin
Pubblicato in: Chemistry – A European Journal, Issue 27/49, 2021, Page(s) 12574-12588, ISSN 0947-6539
Editore: John Wiley & Sons Ltd.
DOI: 10.1002/chem.202101421

Direct 17 O Isotopic Labeling of Oxides Using Mechanochemistry

Autori: Chia-Hsin Chen, Emeline Gaillard, Frédéric Mentink-Vigier, Kuizhi Chen, Zhehong Gan, Philippe Gaveau, Bertrand Rebière, Romain Berthelot, Pierre Florian, Christian Bonhomme, Mark E. Smith, Thomas-Xavier Métro, Bruno Alonso, Danielle Laurencin
Pubblicato in: Inorganic Chemistry, 2020, ISSN 0020-1669
Editore: American Chemical Society
DOI: 10.1021/acs.inorgchem.0c00208

Cost-efficient and user-friendly 17 O/ 18 O labeling procedures of fatty acids using mechanochemistry

Autori: Jessica Špačková, Charlyn Fabra, Guillaume Cazals, Marie Hubert-Roux, Isabelle Schmitz-Afonso, Ieva Goldberga, Dorothée Berthomieu, Aurélien Lebrun, Thomas-Xavier Métro, Danielle Laurencin
Pubblicato in: Chemical Communications, Issue 57/55, 2021, Page(s) 6812-6815, ISSN 1359-7345
Editore: Royal Society of Chemistry
DOI: 10.1039/d1cc02165f

Looking into the dynamics of molecular crystals of ibuprofen and terephthalic acid using 17O and 2H NMR analyses

Autori: Chia‐Hsin Chen, Ieva Goldberga, Philippe Gaveau, Sébastien Mittelette, Jessica Špačková, Chuck Mullen, Ivan Petit, Thomas‐Xavier Métro, Bruno Alonso, Christel Gervais, Danielle Laurencin
Pubblicato in: Magnetic Resonance in Chemistry, 2021, ISSN 1097-458X
Editore: John Wiley & Sons Ltd
DOI: 10.1002/mrc.5141

Operando acoustic analysis: a valuable method forinvestigating reaction mechanisms inmechanochemistry

Autori: Cesar Leroy, Sebastien Mittelette, Gautier Felix, Nicolas Fabregue, Jessica Spackova, Philippe Gaveau, Thomas-Xavier Metro, Danielle Laurencin
Pubblicato in: Chemical Science, 2022, ISSN 2041-6520
Editore: Royal Society of Chemistry
DOI: 10.1039/d2sc01496c

<sup>17</sup>O solid state NMR as a valuable tool for deciphering reaction mechanisms in mechanochemistry: the case study on the <sup>17</sup>O-enrichment of hydrated Ca-pyrophosphate biominerals

Autori: Ieva Goldberga; Nicholai D. Jensen; Christèle Combes; Frédéric Mentink-Vigier; Xiaoling Wang; Ivan Hung; Zhehong Gan; Julien Trébosc; Thomas-Xavier Métro; Christian Bonhomme; Christel Gervais; Danielle Laurencin
Pubblicato in: Faraday Discussions, Issue 241, 2022, Page(s) 250–265, ISSN 1359-6640
Editore: Royal Society of Chemistry
DOI: 10.1039/d2fd00127f

Unveiling the Structure and Reactivity of Fatty-Acid Based (Nano)materials Thanks to Efficient and Scalable 17 O and 18 O-Isotopic Labeling Schemes

Autori: Jessica Špačková, Charlyn Fabra, Sébastien Mittelette, Emeline Gaillard, Chia-Hsin Chen, Guillaume Cazals, Aurélien Lebrun, Saad Sene, Dorothée Berthomieu, Kuizhi Chen, Zhehong Gan, Christel Gervais, Thomas-Xavier Métro, Danielle Laurencin
Pubblicato in: Journal of the American Chemical Society, Issue 142/50, 2020, Page(s) 21068-21081, ISSN 0002-7863
Editore: American Chemical Society
DOI: 10.1021/jacs.0c09383

Fast and Cost‐Efficient <sup>17</sup> O‐Isotopic Labeling of Carboxylic Groups in Biomolecules: From Free Amino Acids to Peptide Chains

Autori: Jessica Špačková; Ieva Goldberga; Rishit Yadav; Guillaume Cazals; Aurélien Lebrun; Pascal Verdié; Thomas‐Xavier Métro; Danielle Laurencin
Pubblicato in: Chemistry - A European Journal, Issue 29, 2022, Page(s) e202203014, ISSN 1521-3765
Editore: Wiley-VCH GmbH
DOI: 10.1002/chem.202203014

First Direct Insight into the Local Environment and Dynamics of Water Molecules in the Whewellite Mineral Phase: Mechanochemical Isotopic Enrichment and High-Resolution 17O and 2H NMR Analyses

Autori: Ieva Goldberga, Nicolas Patris, Chia-Hsin Chen, Emilie Thomassot, Julien Trébosc, Ivan Hung, Zhehong Gan, Dorothée Berthomieu, Thomas-Xavier Métro, Christian Bonhomme, Christel Gervais, Danielle Laurencin
Pubblicato in: The Journal of Physical Chemistry C, 2022, ISSN 1932-7447
Editore: American Chemical Society
DOI: 10.1021/acs.jpcc.2c02070

Induction-heated ball-milling: a promising asset for mechanochemical reactions

Autori: Gautier Félix; Nicolas Fabregue; César Leroy; Thomas-Xavier Métro; Chia-Hsin Chen; Danielle Laurencin
Pubblicato in: Phys Chem chem Phys EISSN: 1463-9084, Issue 1, 2023, ISSN 1463-9076
Editore: Royal Society of Chemistry
DOI: 10.1039/d3cp02540c

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