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Mechanochemistry: a unique opportunity for oxygen isotopic labelling and NMR spectroscopy

Publikacje

From Operando Raman Mechanochemistry to “NMR Crystallography”: Understanding the Structures and Interconversion of Zn-Terephthalate Networks Using Selective 17O‑Labeling

Autorzy: César Leroy, Thomas-Xavier Métro, Ivan Hung, Zhehong Gan, Christel Gervais, Danielle Laurencin
Opublikowane w: Chemistry of Materials, 2022, ISSN 0897-4756
Wydawca: American Chemical Society
DOI: 10.1021/acs.chemmater.1c04132

Probing oxygen exchange between UiO‐66(Zr) MOF and water using <sup>17</sup>O solid‐state NMR

Autorzy: Florian Venel; Raynald Giovine; Danielle Laurencin; Jessica Špačková; Sébastien Mittelette; Thomas‐Xavier Métro; Christophe Volkringer; Olivier Lafon; Frédérique Pourpoint
Opublikowane w: https://hal.univ-lille.fr/hal-04480095, Issue 1, 2024, ISSN 0947-6539
Wydawca: John Wiley & Sons Ltd.
DOI: 10.1002/chem.202302731

Solvent-free synthesis of zeolites: New insights into the mechanism and non-mechanochemical route

Autorzy: Shadi Al-Nahari; Danielle Laurencin; Bruno Alonso
Opublikowane w: Microporous and Mesoporous Materials, Issue 350, 2023, Page(s) 112445, ISSN 1387-1811
Wydawca: Elsevier BV
DOI: 10.1016/j.micromeso.2023.112445

Labeling and Probing the Silica Surface Using Mechanochemistry and 17 O NMR Spectroscopy**

Autorzy: Chia‐Hsin Chen, Frederic Mentink‐Vigier, Julien Trébosc, Ieva Goldberga, Philippe Gaveau, Emilie Thomassot, Dinu Iuga, Mark E. Smith, Kuizhi Chen, Zhehong Gan, Nicolas Fabregue, Thomas‐Xavier Métro, Bruno Alonso, Danielle Laurencin
Opublikowane w: Chemistry – A European Journal, Issue 27/49, 2021, Page(s) 12574-12588, ISSN 0947-6539
Wydawca: John Wiley & Sons Ltd.
DOI: 10.1002/chem.202101421

Direct 17 O Isotopic Labeling of Oxides Using Mechanochemistry

Autorzy: Chia-Hsin Chen, Emeline Gaillard, Frédéric Mentink-Vigier, Kuizhi Chen, Zhehong Gan, Philippe Gaveau, Bertrand Rebière, Romain Berthelot, Pierre Florian, Christian Bonhomme, Mark E. Smith, Thomas-Xavier Métro, Bruno Alonso, Danielle Laurencin
Opublikowane w: Inorganic Chemistry, 2020, ISSN 0020-1669
Wydawca: American Chemical Society
DOI: 10.1021/acs.inorgchem.0c00208

Cost-efficient and user-friendly 17 O/ 18 O labeling procedures of fatty acids using mechanochemistry

Autorzy: Jessica Špačková, Charlyn Fabra, Guillaume Cazals, Marie Hubert-Roux, Isabelle Schmitz-Afonso, Ieva Goldberga, Dorothée Berthomieu, Aurélien Lebrun, Thomas-Xavier Métro, Danielle Laurencin
Opublikowane w: Chemical Communications, Issue 57/55, 2021, Page(s) 6812-6815, ISSN 1359-7345
Wydawca: Royal Society of Chemistry
DOI: 10.1039/d1cc02165f

Looking into the dynamics of molecular crystals of ibuprofen and terephthalic acid using 17O and 2H NMR analyses

Autorzy: Chia‐Hsin Chen, Ieva Goldberga, Philippe Gaveau, Sébastien Mittelette, Jessica Špačková, Chuck Mullen, Ivan Petit, Thomas‐Xavier Métro, Bruno Alonso, Christel Gervais, Danielle Laurencin
Opublikowane w: Magnetic Resonance in Chemistry, 2021, ISSN 1097-458X
Wydawca: John Wiley & Sons Ltd
DOI: 10.1002/mrc.5141

Operando acoustic analysis: a valuable method forinvestigating reaction mechanisms inmechanochemistry

Autorzy: Cesar Leroy, Sebastien Mittelette, Gautier Felix, Nicolas Fabregue, Jessica Spackova, Philippe Gaveau, Thomas-Xavier Metro, Danielle Laurencin
Opublikowane w: Chemical Science, 2022, ISSN 2041-6520
Wydawca: Royal Society of Chemistry
DOI: 10.1039/d2sc01496c

<sup>17</sup>O solid state NMR as a valuable tool for deciphering reaction mechanisms in mechanochemistry: the case study on the <sup>17</sup>O-enrichment of hydrated Ca-pyrophosphate biominerals

Autorzy: Ieva Goldberga; Nicholai D. Jensen; Christèle Combes; Frédéric Mentink-Vigier; Xiaoling Wang; Ivan Hung; Zhehong Gan; Julien Trébosc; Thomas-Xavier Métro; Christian Bonhomme; Christel Gervais; Danielle Laurencin
Opublikowane w: Faraday Discussions, Issue 241, 2022, Page(s) 250–265, ISSN 1359-6640
Wydawca: Royal Society of Chemistry
DOI: 10.1039/d2fd00127f

Unveiling the Structure and Reactivity of Fatty-Acid Based (Nano)materials Thanks to Efficient and Scalable 17 O and 18 O-Isotopic Labeling Schemes

Autorzy: Jessica Špačková, Charlyn Fabra, Sébastien Mittelette, Emeline Gaillard, Chia-Hsin Chen, Guillaume Cazals, Aurélien Lebrun, Saad Sene, Dorothée Berthomieu, Kuizhi Chen, Zhehong Gan, Christel Gervais, Thomas-Xavier Métro, Danielle Laurencin
Opublikowane w: Journal of the American Chemical Society, Issue 142/50, 2020, Page(s) 21068-21081, ISSN 0002-7863
Wydawca: American Chemical Society
DOI: 10.1021/jacs.0c09383

Fast and Cost‐Efficient <sup>17</sup> O‐Isotopic Labeling of Carboxylic Groups in Biomolecules: From Free Amino Acids to Peptide Chains

Autorzy: Jessica Špačková; Ieva Goldberga; Rishit Yadav; Guillaume Cazals; Aurélien Lebrun; Pascal Verdié; Thomas‐Xavier Métro; Danielle Laurencin
Opublikowane w: Chemistry - A European Journal, Issue 29, 2022, Page(s) e202203014, ISSN 1521-3765
Wydawca: Wiley-VCH GmbH
DOI: 10.1002/chem.202203014

First Direct Insight into the Local Environment and Dynamics of Water Molecules in the Whewellite Mineral Phase: Mechanochemical Isotopic Enrichment and High-Resolution 17O and 2H NMR Analyses

Autorzy: Ieva Goldberga, Nicolas Patris, Chia-Hsin Chen, Emilie Thomassot, Julien Trébosc, Ivan Hung, Zhehong Gan, Dorothée Berthomieu, Thomas-Xavier Métro, Christian Bonhomme, Christel Gervais, Danielle Laurencin
Opublikowane w: The Journal of Physical Chemistry C, 2022, ISSN 1932-7447
Wydawca: American Chemical Society
DOI: 10.1021/acs.jpcc.2c02070

Induction-heated ball-milling: a promising asset for mechanochemical reactions

Autorzy: Gautier Félix; Nicolas Fabregue; César Leroy; Thomas-Xavier Métro; Chia-Hsin Chen; Danielle Laurencin
Opublikowane w: Phys Chem chem Phys EISSN: 1463-9084, Issue 1, 2023, ISSN 1463-9076
Wydawca: Royal Society of Chemistry
DOI: 10.1039/d3cp02540c

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